GCMS analysis log for sample AD30713, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC3101\30713.D Vial: 28 Acq On : 1 Jan 2002 3:07 pm Operator: 209 GALOS Sample : gems Scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

11.13 1.27 ug/1 363659 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 86 2 2-Oxo-4-pheny1-6- (4-chlorophenyl) -1 282 C16H11C1N2O 000000-00-0 9 3 6,7-Benzo-Dhenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 9 4 Benzene, 1phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 9 Abundance Scan 663 (11.134 min): 30713.0 (-) m/z 281.00 100.00% 2111

5000 . n ... 10.80 11.00 11.20 11.40

miz-> .45, 59 7,89 103 119 133,147 163 177 113,297 221 235 249, 265. . , | 40 60 ' 80 100 120 140' 160 180 200 220 240 260 280 m/z 282.00 27.61% Abundance #41966: Cyclotetrasiloxane, octamethyl- 281

5000 10.80 11.00 11.20 11.40 ‘ ' m/z 283.00 16.44% 133 ■ ‘ i 1 ‘ 73 163 177 191 I 207 235 249 265 I ”11 ‘' ■ • 1 ■ ‘ i ■ ■ ■ ■ I ‘ 1 ■ ‘ i 1 • • ■ i • ' • ■ i ■ • ■ ■ i ■ ■ ■ •' i ‘ • 1 ■ i। ■r ‘ ■ i • ■1 ■ । miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39756:2-Oxo-4-phenyl-6-(4-chlorophenyl)-1 2-dihydropyrimi 281 • 1 i ' • ■ ‘ I ‘ ‘ 1 i • • • ■ i ■ • 1 • i 10.80 11.00 11.20 11.40 5000 m/z 192.90 10.62% j 102 123 141 175 204 1 247 TIPTIWBTTTTT ■ ■ i ■ ■ • ‘ i ■1 ■ ■ i ■ • ■ • i1 • ■ • t ■1 ‘ ■ i ‘1 • • i • ■ '' i ■ ■ ■ • i m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39602:6,7-Benzo-phenothiazine-5,5-dioxide T 1 I I I J } r I ! | I 11 I । I i ii F 281 10.80 11.00 11.20 11.40 I m/z 73.00 10.06% 5000 217 I 232 ,

m/z-> 1 118.199.204, ..M 252264. ■ ■ 40 60 80 100 120 140 160 180 200 220 240 260 280 , ----- ARYT 10.80 11.00 11.20 11.40

30713.D GCMS1126.M Wed Jan 23 08:46:22 2002 Page 2

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