Automated laboratory log recording GCMS analysis of sample AD30695 including detection of unknown compounds and surrogates.
NYC-WTC_000018107–000018122Folder label: “GCMS X 12/27/01 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30695.D Vial: 32 Acq On 1 Jan 2002 6:59 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T.
11.13 1.17 ug/1 273954 1,4-Dichlorobenzene-d4 11.68
Hit# Of 5 Tentative ID MW MolForm CAS# Qual
l Cyclotetrasiloxane, octamethyl- 296 C8H2404Si4 000556-67-2 64 2 2-Oxo-4-pheny1-6- (4-chlorophenyl)-1 282 C16H11C1N2O 000000-00-0 9 3 6,7-Benzo-phenothiazine-5, 5-dioxide 281 C16H11NO2S 000000-00-0 9 4 Benzene,y/l-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 9 Abundance / Scan 663 (11.127 mln): 30695.D(-) m/z 281.00 1 00.00% 201
5000
45 59 73 | 133 88 103 119, I 147 163 177 193 207 249 265 10.80 11.00 11.20 11.40 ' -221,239— 4 J pt’i 1 I* f l ll rrri l | ri "I rr ? J Mgr r ITP’ri J "r m/z 282.00 30.82% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #72646: Cyclotetrasiloxane, octamethyl- 281
5000 10.80 11.00 11.20 11.40 ' ‘1 79 265 m/z 283.0,0 17.72% 45 59 j 133 L 177 193 207 235 ’’I****I*+-I****I5*’I**’-1***I****1*’*11**1* ■' • < f‘ ■ m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39756: 2-Oxo-4-phenyl-6-(4-chlorophenyl)-1.2-dihydropyrimi 251 । ‘«• "i I i' 11 r i->- > 11 i i' 111 10.80 11.00 11.20 11.40 5000 m/z 192.90 12.33%
102 123 141 175 204 247 i T*1uu————uu—3—uiouoornn]tun —ng—um—u—igrr miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39602:6,7-Benzo-phenothiazine-5, 5-dioxide **1’**I’*’I’’1444*I 281 10.80 11.00 11.20 11,40 m/z 133.0.0 11.70% 5000 217 232 102 ng 189 294 TTIPTIAAIIPPTI . ,252264. ‘ I** 1 ' i ‘ ‘ ' i miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 10.80 11.00 11.20 11.40
30695.D GCMS1126.M Wed Jan 23 08:33:29 2002 Page 2
NYC-WTC_000018115
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NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018093
Automated laboratory log recording GCMS analysis of sample AD30694 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018624
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30904 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018754
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036842
GCMS analysis report for sample AD29670 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036542
Laboratory commentary noting detection of bis(2-Ethylhexyl)phthalate in sample AD29520 and blank on January 25, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018058
Document with unreadable text from the GCMS X folder series in DEP Box 16.
Filed in the same folder
NYC-WTC_000018059
Calibration verification report using DFTPP standard for GCMS instrument performance check on January 1, 2002.
Filed in the same folder
NYC-WTC_000018060
Laboratory report documenting GCMS calibration analysis of sample AD30694 conducted on January 18, 2002.
Filed in the same folder
NYC-WTC_000018064
Reference data table listing response factors and concentrations for organic compounds used in GCMS analysis of sample AD30694.
Filed in the same folder
NYC-WTC_000018069
Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.
Filed in the same folder