GCMS analysis log for sample AD30712, Jan 2002

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Data File C:\HPCHEM\ 1\DATA\DEC3101\30712.D Vial: 35 Acq On 1 Jan 2002 9:53 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T. 11.13 3.49 ug/1 718934 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4S14 000556-67-2 74 2 2-Oxo-4-phenyl-6- (4-chlorophenyl) -1 282 C16H11C1N2O 000000-00-0 9 3 6,7-Benzo-phenothiazine-5, 5-dioxide 281 C16H11NO2S 000000-00-0 9 43,6-Bis(N-dimethylamino)-9-ethylcar281C18H23N3 Abundance Scan 662 (11.125 min): 30712.D (-) 057103-04-5 9 m/z 281.00 100.00% 211

5000 *1*’*I’*I*’’’I 6 ‘ I 45 59 73 89 103 119/123 147 163 177 123 207 221 235 249 2®5 [ 10.80 11.00 11.20 1140 1 I | i' I i ry i 1 M I r r . I । 'I .1 1 I i 1** । T . . IT , "Ti । 'rt . , । . .1 । . " . j rt , , ft m/z 282.00 27.93% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 281

5000 m 10.80 11.00 11.20 11.40 m/z 283.00 17.56% 73 133 .0 207 I 163 177 191 1. 235 249 265

1 ■1 ■ I ■1111 ■ ‘ • • i" • miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39756; 2-Oxo-4-phenyl-6-(4-chlorophenyl)-1,2-dihyd ropyrimi 281 4 ■ i • ■ ' ■ i 10.80 11.00 11.20 11.40 5000 m/z 192.90 12.26% ..................... ;

102 123 141 175 204 247 ‘I ' 1 ' 1 1“ ' ' f 1 " 1 ' 1 1 rl 1 1 1 ' 1 Wr ■ • 11 ■ ' 1 ' i 1 ■ ' 1 i ■ ■ • ■ i ‘ ‘ • 1 i ■ 1 ■ ■ i ■ • ■ ' t ‘ miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39602:6,7-Benzo-phenothiazine-5,5-dioxide 1. I ‘ ‘ j » • » i l . . » » I ...» j 281 10.80 11.00 11.20 11.40 m/z 133.00 11.41% 5000 217 232 102 118 189 204 , : —1210—01252264 I * » * । * ‘ * ' t * 1 ’*1***1 miz-> 40 60 80 100 120 140 160 180 200 220 240। 260 280 10.80 11.00 11.20 11.40

30712 .D GCMS1126.M Wed Jan 23 08:42:30 2002 Page 2

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