Laboratory report documenting GCMS analysis of sample AD31018 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.
NYC-WTC_000017380–000017404Folder label: “GCMS X 12/20/01 A 1/8/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C: \HPCHEM\Y 1 \DATA\ JAN0 802\31018.D Vial: 14 Acq On 9 Jan 2002 2:01 am Operator: 209 GALOS Sample gems scan 12/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T. 10.99 3.21 ug/1 731576 1,4-Dichlorobenzene-d4 11.53 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotetrasi xane, octamethyl- 296 C8H24O4Si4 000556-67-2 38 2 2-Oxo-4-pheniyl-6-(4-chlorophenyl)-1 282 C16H11C1N2O 000000-00-0 9 3 6,7-Benzo-phenothiazine-5, 5-dioxide 281 C16H11NO2S 000000-00-0 9 4 3,6-Bis‘N-dimethylamino) -9-ethylcar 281 C18H23N3 057103-04-5 9 Abundance 7 ” Scan 648 (10.993 irhln): 31018.D (-) p 100.00% 281
5000
11’1143 1 ' I ' 1 ' ' I 1 1 10.60 10.80 11.00 11.20 11.40
m/z-> 4s 59 73 , 89 103 119 133147 163 177 13207 221 235 249 2h. . , i I TTI ITT44 l“l f l'T > I l Y l"l TT r i 111 | ■ T I I TT 1 1 "I 1 11 ...... III-‘‘I‘ ‘ 1 | ‘1 1 i f Pr m/z 282.00 28.13% 40 60 _ 80__100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 281
5000 10.60 10.80 11.00 11.20 1140 m/z 283.00 18.00% 73 133 0 207 235 249 265 I 163 177 191 | mte~> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance 281 •" 111 " “ i " 10.60 10.80 11.00 11.20 11.40 5000 m/z 192.90 12.98%
102 123 141 175 204 247 m/z-> 40 ' ‘ 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39602:6,7-Benzo-phenothiazine-5,5-dioxide 281 10.60 10.80 11.00 11.20 11.40 m/z 133.00 12.50% 5000 217 232 102 118 189 204 | . , [I,) .252264 ■ ■ । ‘ • i1 ■ ■ ■ । ■ ----- m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 10.60 10.80 11.00 11.20 11.40
31018.D GCMS0103.M Wed Jan 09 12:07:36 2002 Page 2
NYC-WTC_000017388
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NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016096
GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017405
Laboratory report documenting GCMS analysis of sample AD31074 conducted on January 18, 2002, noting no unusual compounds were detected.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018693
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018754
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018214
Automated laboratory log recording GCMS analysis of sample AD30712 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036656
Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000017329
Document page containing only the CCAS identifier with no readable text or specific content details visible.
Filed in the same folder
NYC-WTC_000017330
Fragmented page from a laboratory method document regarding extraction and analysis procedures for GCMS testing.
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NYC-WTC_000017334
Laboratory report documenting GCMS calibration analysis of sample AD31017 conducted on January 8, 2002, listing concentrations of various organic compounds.
Filed in the same folder
NYC-WTC_000017338
Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31017 performed on January 18, 2002.
Filed in the same folder
NYC-WTC_000017344
Laboratory report listing detection limits for numerous organic compounds in a GCMS blank sample analyzed on January 10, 2002.
Filed in the same folder