Laboratory report documenting GCMS analysis of sample AD31074 conducted on January 18, 2002, noting no unusual compounds were detected.
NYC-WTC_000017405–000017433Folder label: “GCMS X 12/20/01 A 1/8/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\JAN0802\31074.D Vial: 12 Acq On : 9 Jan 2002 12:04 am Operator: 209 GALOS Sample : gems scan 12/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
11.00 3.63 ug/1 961287 1,4-Dichlorobenzene-d4 11.52
Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotetrasiloxane, octamethyl- 000556-67-2 78 296 C8H2404Si4 2 2-Oxo-4-phenyl-6-(4-chlorophenyl)-1 282 C16H11C1N2O 000000-00-0 9 3 6,7-Benz Xphenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 9 4 3,6-Bis{ -dimethylamino)-9-ethylcar 281 C18H23N3 057103-04-5 9 Abundance A Scan 649 (10.999 min): 31074.D (-) m/z 281.00 100.00% 201
5000
10.60 10.80 11.00 11.20 11.40 45 59 73 85 . 103 119 133।1471 'i 1 163 1 1 Tl’’ 1 "TT 1 rt TT ri l T fTT"T 17*1 I’T 1 177 114 । TT , 221 1 II . 123207 > 1 । 249 < j । 1235 j .‘"i . .. ।, r 1 1 . 265 m/z 282.00 28.31% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 281
5000 10.60 10.80 11.00 11.20 11.40 133 207 m/z 283.00 17.01% 73 | 163 177 191 1 235 249 265 | m/z-> 40 60 80 100 120 140 160 180 200 220 '246' 260 280 Abundance 281 ........ l\........... 10.60 10.80 11.00 11.20 1140 5000 m/z 192.90 11.82%
102 123 141 175 204 247 m/z--> 40_ 60__ 80. 100 120 140 160 180 200 220 240 260 280 Abundance #39602: 6,7-Benzo-phenothiazine-5,5-dioxide 281 10.60 10.80 11.00 11.20 11.40 m/z 133.00 10.49% 5000 217 232 102 118 —ImdmmTTm 189 204 252264 ....... l\......... m/z~> 40 60 80 100 120 140 160 180 200 220 240 260 280 10.60 10.80 11.00 11.20 11.40
31074.D GCMS0103.M Wed Jan 09 12:24:19 2002 Page 2
NYC-WTC_000017414
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NYC-WTC_000017380
Laboratory report documenting GCMS analysis of sample AD31018 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018693
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018214
Automated laboratory log recording GCMS analysis of sample AD30712 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016096
GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018754
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018005
Laboratory report listing PAHs and phthalates in a water sample scheduled for re-extraction and re-analysis.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036656
Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000017329
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Filed in the same folder
NYC-WTC_000017330
Fragmented page from a laboratory method document regarding extraction and analysis procedures for GCMS testing.
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NYC-WTC_000017334
Laboratory report documenting GCMS calibration analysis of sample AD31017 conducted on January 8, 2002, listing concentrations of various organic compounds.
Filed in the same folder
NYC-WTC_000017338
Record of a gas chromatography-mass spectrometry run for unknown compounds in sample AD31017 performed on January 18, 2002.
Filed in the same folder
NYC-WTC_000017344
Laboratory report listing detection limits for numerous organic compounds in a GCMS blank sample analyzed on January 10, 2002.
Filed in the same folder