GCMS analysis results for sample AD29667, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

• Data File . : C:\HPCHEM\l\DATA\DEC3101\29667.D Vial: 56 Acq On : 2 Jan 2002 8:14 pm Operator: 209 GALOS Sample : gems scan 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

11.13 0.77 ug/1 321307 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 78 2 2-Oxo-4-phenyl-6/(4-chlorophenyl)-1 282 C16H11C1N2O 000000-00-0 9 3 6 , 7-Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 9 4 3,6-Bis (N-dimethylamino) -9-ethylcar 2 81 C18H23N3 057103-04-5 9 Abundance 7 Scan 663 (11.129 min): 29667.D (-) m/z 281.00 100.00% 281

5000 ............ / 733 _ 132 193 20- 240 265 10.80 11.00 11.20 11.40_____ 45 59 1 89 103 119 | 147 163 177 II, 4 221 235 L “2 W-r m/z 282.00 28.18% mlz-> 40 60 (80 100 120 140 160 180 20G 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 281

5000 - 10.80 11.00 11.20 11.40 m/z 283.00 17.23% 73 133 .. 207 | 163 177 191 | 235 249 265 m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39756; 2-Oxo-4-phenyl-6-(4-chlorophenyl)-1,2-dihydropyrimi 281 I i ■ i ’ ■ ■ ■ i 10.80 11.00 11.20 11.40 5000 - m/z 192.90 11.57%

102 123 141 175 204 247 m/z-> Abundance 40 ' i ■ ' ' ■ i 1 ■ ■ ■ i ■ 60 80 100 120 140 160 180 200 #39602: 6.7-Benzo-phenothiazine-5,5-dioxide 220 240 260 280

281 ..... A..... 10.80 11.00 11.20 11.40

JIB m/z 73.00 10. 97% 5000 217 232 102 118 189 204 252264 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 10.80 11.00 11.20 11.40

29667.D GCMS1126.M Wed Jan 16 14:47:43 2002 Page 2

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