NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Document / 23 pages
GC/MS analysis results for sample AD30909, Jan 28 2002
Machine-extracted title · confidence 100%Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
NYC-WTC_000018693–000018715Folder label: “GCMS X 12/19/01 A 1/2/02”
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NYC 9/11 Public Portal Document
Library Search Compound Report Data File C:\HPCHEM\ 1\DATA\DEC3101\30909.D Vial: 52 Acq On 2 Jan 2002 4:19 pm Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T. 11.13 0.57 ug/1 126997 1,4-Dichlorobenzene-d4 11.68 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 78 2 2-Oxo-4-phenyl-6-(4-chlorophenyl)-1 282 C16H11C1N2O 000000-00-0 9 3 6,7-Benzo-phenothiazine- 5,5-dioxide 281 C16H11NO2S 000000-00-0 9 4 3,6-Bi^(N-dimethylamino)-9-ethylcar 281 C18H23N3 057103-04-5 9 (Abundance Scan 663 (11.133 mln): 30909.D (-) m/z 281.00 100.00% 281
5000
' 1 I F‘ 1 • I 73 10.80 11.00 11.20 11.40 i 45 59 | I TIWTTgT 88 103,119133 147 ,163 177 13297 ।, 235 249 |2/5, er m/z 282.00 2 9.06% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 28 1
5000 10.80 11.00 11.20 1140 ‘ ' 133 m/z 283.00 17.71% 73 163 177 191 207 . or i I 235 249 265 | • ■ i ■ ■ ■ ■ i • ■ • 1 i ■ • ■ • i • ‘ •1 i 1 ■ • ■ i ■ • • ■ i ■ ■ ■ • i ■ ■ ■ • i m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39756: 2-Oxo-4-phenyl-6-(4-chloraphenyl)-1 2-dihydropyrimi 281 **I**** 14/41/8//* t 10.80 11.00 11.20 11.40 5000 m/z 192.90 12.36%
102 123 141 175 204 247 I4mo————u———B—anpBBa/IIVV“HBBIIIIIIIBIEIFT7ET4}+/44gt miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39602:6,7-Benzo-phenothiazine-5,5-dioxide 1 1 I 1 1 1 1 I 1 1 1 1 I ■ 1 1 ‘ I 281 10.80 11.00 11.20 11.40 m/z 133.00 10.74% 5000 217 232 102 118 189 294 5*1*’*1**--4-411******* Y7H44252284 1111 ’AI* I 4 11 1 1 1 1 1 ' i 1 1 1 1 1 miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 10.80 11.00 11.20 11.40
30909.D GCMS1126.M Fri Jan 25 11:40:05 2002 Page 2
NYC-WTC_000018701
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