Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
NYC-WTC_000018174–000018193Folder label: “GCMS X 12/27/01 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30714.D Vial: 29 Acq On 1 Jan 2002 4:05 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
11.13 1.64 ug/1 442905 1,4-Dichlorobenzene-d4 11.67
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclotetrasiloxane, octamethyl - 296 C8H2404Si4 000556-67-2 83 2 6,7-Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 9 3 3,6-Bis(N-dimethylamino)-9-ethylcar 281 C18H23N3 057103-04-5 9 4 Benzene, l^-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 9 Abundance Scan 663 (11.130 min): 30714.D (-) m/z 281.00 100.00% 281
5000 / V 10.80 11.00 1120 11.40 45 59 73 . 89 103 119 133147 163 177 13 207 221/235 249 J". I’I’’’47’* n I T’TIT "T"I ’ j vi 1’4 j FT’ » Q » in t vt j i । j i । t । । Cru nn m/z 282.00 27.53% miz-> 40 60 80 100 120 140 .160 180 200 220 240 260 Abundance #41966: Cyclotetrasiloxane, octamethyl- 281
5000 10.80 11.00 11.20 11.40 ' 207 > m/z 283.00 17.95% 73 133 I I 163 177 191 | 235 249 265 | ■ • i ■ ■ ■ • i ‘ ' i' • ■ • i ‘1 ■ • i ■ • ■ • i • BBmnB—DOmTmuaaa —TmBSTTT 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39602; 6,7-Benzo-phenothiazine-5,5-dioxide 281
10.80 11,00 11.20 11.40 5000 m/z 192.9,0 11.70%
102 118 217232। •252264 189 204 | TIIuaunuo——n—nfuu—potpn‘u—nmotTeupunttvr miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39624:3,6-Bis(N-dimethylamino)-9-ethylcarbazole / \ T i ■ • • • I T T 281 10.80 11.00 11.20 11.40 m/z 133.00 11.33% 5000 266
141 208 222 237 250 , | ‘*1**1***I***I‘‘‘‘I miz-s 40 60 80 100 120 140 160 180 200 220 240 260 280 10.80 11.00 11.20 11.40
30714.D GCMS1126.M Wed Jan 23 08:49:53 2002 Page 2
NYC-WTC_000018182
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NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018754
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018693
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018214
Automated laboratory log recording GCMS analysis of sample AD30712 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016096
GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036656
Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018058
Document with unreadable text from the GCMS X folder series in DEP Box 16.
Filed in the same folder
NYC-WTC_000018059
Calibration verification report using DFTPP standard for GCMS instrument performance check on January 1, 2002.
Filed in the same folder
NYC-WTC_000018060
Laboratory report documenting GCMS calibration analysis of sample AD30694 conducted on January 18, 2002.
Filed in the same folder
NYC-WTC_000018064
Reference data table listing response factors and concentrations for organic compounds used in GCMS analysis of sample AD30694.
Filed in the same folder
NYC-WTC_000018069
Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.
Filed in the same folder