GCMS analysis log for sample AD30694, Jan 2002

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Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC3101\30694.D Vial: 31 Acq On 1 Jan 2002 6:01 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table . Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 11.13 0.65 ug/1 156951 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclotetrasiloxane, octamethyl- 296 C8H2404S14 000556-67-2 56 2 3,6-Bis(N-dimethylamino) -9-ethylcar 281 C18H23N3 057103-04-5 25 3 2-Oxo-4-phenyl-6- (4-chlorophenyl)-1 282 C16H11C1N2O 000000-00-0 9 4 6,7-Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 9

I . Abundance Scan 663 (11.129 min): 30694.D (-) m/z 281.00 1 00.00% 281

5000

i | miz-> Abundance 45 59 I 71 89 103 119 133 147 163 177 123 297 235 249 225 1 1 1 I ‘'r 1 11 1 1 11 1 1i T i I I’t j 'i ,i“‘| । » । » [ । *i j r V r i “prrri । ff ! i । i । i *i1 j FTT" r । 1i j r ] 40 60 80 100 120 140 160 180 200 220 #72646: Cyclotetrasiloxane, octamethyl- 240 260 280 m/z 7 10.80 11.00 11.20 11.40 ‘1 29.66%

2511

/ 5000 T i 1 • T T T 10.80 11.00 11.20 11.40 265 m/z 283.00 15.22% 7 133 45 59 । t 177 193 297 235 L * • । • •1 * (1 •1 ‘ । ’ ’ • • i * • * n •1 * • । • * • * । * • ‘ • i * • • * । *k • * ।11 * * i * * • * i ’ *»* ।»* 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39624; 3.6-Bis(N-dimethylamino)-9-ethylcarbazole 281 ■ ■ i 1 1 ■ ' i ■ • • i ■ • ■ • i 10.80 11.00 11.20 11.40 5000 m/z 192.90 12.54% 266

• 141 208 222 237 250 TT । r > i i । । । m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39756:2-Oxo-4-phenyl-6-(4-chlorophenyl)-1,2-dihydropyrimi 1 ■ i ■ ■ T-r-p-r-n-f 281 10.80 11.00 11.20 11.40 m/z 133.00 10.82% 5000

102 123 141 175 204 1*—2,0,/t2B3—1———*numuDmuTamummmPgf 247 | VV 88s । > • i j । i 4**t 1 1 11 | miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 10.80 11.00 11.20 11.40

30694.D GCMS1126.M Wed Jan 23 08:31:10 2002 Page 2

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