Automated laboratory log recording GCMS analysis of sample AD30711 including detection of unknown compounds and surrogates.
NYC-WTC_000018142–000018154Folder label: “GCMS X 12/27/01 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30711.D Vial: 34 Acq On 1 Jan 2002 8:55 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
11.13 0.57 ug/1 137739 1,4-Dichlorobenzene-d4 11.68
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclotetrasiloxane, octamethyl- 296 C8H2404Si4 000556-67-2 86 2 Benzene, 1-phenyl-4- (2-cyano-2-phen 281 C21H15N 027869-56-3 47 3 6,7-Bento-phenothiazine-5, 5-dioxide 281 C16H11NO2S 000000-00-0 9 4 3,6- s(N-dimethylamino)-9-ethylcar 281 C18H23N3 057103-04-5 9 Abundance 2 li Scan 663 (11.129 mln): 30711.D (-) ~ m/z 281.^1 100.00% 211
5000
45 59 73 88 103 119 133 147 163 179 123 207 235 249 265 10.80 11.00 11.20 11.40
.. t 11 n l n' i-i । । A fi f1‘ *r*i ITT it, ■ i? 11 *l । fT Ti ‘1′4114 ... । A .. । +rr 27.45% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 281
■11 ■ ■ ■ ■ । 5000 T ) * ’ T 10.80 11.00 11.20 11.40 m/z 283.00 16.63% 133 ' • I ’ ’1 11 ‘ 73 I 163 177 191 207 235 249 285 I ■ i ■ • • ' i ■ ■ ■ • i 1 ■ • • i ■ ‘ ‘ 11 ■ ‘ ‘ '"I 1 ■ ' 11 7/414*/‘‘S* ‘ ‘ * I ‘ ’ I * • m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #.33643, Benzene, 1-phenyl-4-(2-cyano-2-phenyletheny!) 281 • • i • • • • i • > ■ ■ I ■ 1 1 • I 10.80 11.00 11.20 11.40 5000 m/z 192.90 13.26% 126 203 ,253266 I ..124240 ; m/z~> 40 so 80 100 120"140 160"iso 200 '226' 240 260 280 A. A Abundance #39602:6,7-Benzo-phenothiazine-5,5-dioxide 281 10.80 11.00 11.20 11.40'11 m/z 133.00 10.94% 5000 217 232 102 118 189 204 . 252264 L 1I0]0mmmmmTr • •!*»•»p • miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 10.80 11.00 11.20 11.40TU1
30711.D GCMS1126.M Wed Jan 23 08:38:58 2002 Page 2
NYC-WTC_000018150
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NYC-WTC_000018093
Automated laboratory log recording GCMS analysis of sample AD30694 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018650
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30906 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018248
Laboratory report documenting GCMS analysis of sample AD30984 conducted on January 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018107
Automated laboratory log recording GCMS analysis of sample AD30695 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016783
GCMS analysis of environmental sample AD30118 conducted January 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017478
Laboratory report documenting GCMS analysis of sample AD31075 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049762
GCMS analysis report for sample AD31640 conducted on February 11, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049734
GCMS analysis report for sample AD31642 conducted on February 11, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036831
Gas chromatography-mass spectrometry analysis of sample AD29666 identifying unknown compounds and surrogate recovery data (2,4-DDD at 72%), January 28, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036815
GCMS analysis report for sample AD29667 listing unknown compounds and surrogate recovery data from January 28, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018058
Document with unreadable text from the GCMS X folder series in DEP Box 16.
Filed in the same folder
NYC-WTC_000018059
Calibration verification report using DFTPP standard for GCMS instrument performance check on January 1, 2002.
Filed in the same folder
NYC-WTC_000018060
Laboratory report documenting GCMS calibration analysis of sample AD30694 conducted on January 18, 2002.
Filed in the same folder
NYC-WTC_000018064
Reference data table listing response factors and concentrations for organic compounds used in GCMS analysis of sample AD30694.
Filed in the same folder
NYC-WTC_000018069
Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.
Filed in the same folder