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GCMS analysis log for sample AD30711, Jan 2002

Machine-extracted title · confidence 100%

Automated laboratory log recording GCMS analysis of sample AD30711 including detection of unknown compounds and surrogates.

NYC-WTC_000018142–000018154

Folder label: “GCMS X 12/27/01 A 1/16/02

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C: \HPCHEM\ 1 \DATA\DEC3101\30711.D Vial: 34 Acq On 1 Jan 2002 8:55 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.62 3.04 ug/1 736841 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethylformamide 73 C3H7NO 000627-45-2 9 2 Butane, 2-methoxy-2-methyl- 102 C6H140 000994-05-8 9 3 3 -Pentanol , 3 -methyl - 102 C6H140 000077-74-7 9 4 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 Abundance Scan 281 (7.822 mln): 30711.D (-) m/ z 73.00 100.00% 73

5000 43 ---------- --- j i i t f | i t l i j i > X-« | I I < • i • • , ,87 103 7.20 7.40 7.60 7.80 8.00 mptmm l.. j. ’** ।. H l p'l 11 p 111...................................... ,1 1 55 ।।p... t।।11.... 208।... m/ z 43.00 32.14% miz-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #292: N-Ethylformamide 30 73

5000 i ■ ■ ■ ■ i • ■ 1 i । • • < । । i > TTTd 44 58 7.20 7.40 7.60 7.80 8.00 m/z 41.0.0 11.36%

miz-> m unpapun 15 ।....p'l.11।।।।r1...i।.l||।j ... 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #1761: Butane. 2-methoxy-2-methyl- i f 73 7.20 7.40 7.60 7.80 8.00 5000 m/z 45.05 11.29% 55 87 27 45 TTe 11 j». A ri j | . ....’ J...... 1...... ...................................................................... .... JU .. J H .', | I | J .... j 1 j I I I > J I I I I j 1 I I I J I I I m/z-> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #63573:3-Pentanol, 3-methyl- DgmuuBTTTTPm i 73 7.20 7.40 7.60 7.80 8.00 m/z 71.00 7.47% 5000 45 55 27 87 1 . ,i ..... ...... . ...... ............................................................................. .।..n।....|.1..।.।....।....।....।....t।....।....।.i.11..h।....।....।... 1*11* ■.... crAri . miz—> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 7.20 7.40 7.60 7.80 8.00

30711.D GCMS1126.M Wed Jan 23 08:38:53 2002 Page 1

NYC-WTC_000018149

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NYC-WTC_000018149Source: NYC Law Department, mirrored locally

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