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GCMS analysis log for sample AD30695, Jan 2002

Machine-extracted title · confidence 100%

Automated laboratory log recording GCMS analysis of sample AD30695 including detection of unknown compounds and surrogates.

NYC-WTC_000018107–000018122

Folder label: “GCMS X 12/27/01 A 1/16/02

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Scanned page image, NYC-WTC_000018114
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC3101\30695.D vial: 32 Acq On 1 Jan 2002 6:59 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Pentane, 3-methoxy- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.62 3.50 ug/1 817376 1,4-Dichlorobenzene-d4 11.68 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Pentane, 3-methoxy- 102 C6H14O 036839-67-5 25 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 4 Silane, tetramethyl- 88 C4H12Si 000075-76-3. 9 Abundance Scan 281 (7.620 mln): 30695.D (-) m/z 73.00 100.00% 73

5000 43 i ' ■ ■ ■ i ■ 1 1 1 1 1 1 1'14mT 1 1 1 1 ................................... 38.1, . 50 55 go 87 67| 103 7.20 7.40 7.60 7.80 8.00 ■ ■ i ■ ■ ' ■ i ■ ■ ■ ■ I 1 1 1 1 I1 11 1 I' 1 1 । 1 1 1 1 1 r1 H I**I**IsiT m/z 43.00 31.11% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1793: Pentane, 3-methoxy- 73

5000 45 7.20 7.40 7.60 7.80 8.00 ' m/z 41.00 12.23%

miz-> .......... 27 3033 39, • » i • • » • i • > • * i • • • ■ t i . ■ ■ i ■ 55 ■ i ■ . . . j'i I ■ • i ' 1 ' ■ i • ■ 1 1 i 1 1 ' 1 i 1 10 20 40 50 60 70 80 90 100 110 (Abundance #292: N-Ethylformamide 30 73 । .... I r-i rrJ| 1 |--=4- I—r;| i i i rpr 7.20 7.40 7.60 7.80 8.00 5000 m/z 45.05 11.61% 44 58 15 J i *II***I*I 1 • • i ■ ' ■ ' i ■ ■ ' 1 i 1 ' 1 1 i 1 :m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #763: 1-Butanamine, 3-methyl- I • • •*r J . | . mma . 30 7.20 7.40 7.60 7.80 8.00 m/z 71.00 7.15% 5000

15 41 55 70 87 J ■ ■ । ■ i ■ ■ 1 ■ 1’1 I I 1 ' ■ ■ i ‘ ‘ ■ i ■ ■ ' ■ i ' • ■ ■ i • 1 miz-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80 8.00

30695.D GCMS1126.M Wed Jan 23 08:33:24 2002 Page 1

NYC-WTC_000018114

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NYC-WTC_000018114Source: NYC Law Department, mirrored locally

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