GCMS results for unknowns, sample AD31217, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\JAN0902 \31217.D Vial: 24 Acq On : 10 Jan 2002 1:33 pm Operator: 209 GALOS Sample : gems scan 12/21 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.47 2.96 ug/1 825631 1,4-Dichlorobenzene-d4 11.53

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H14O 000077-74-7 33 2 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 3 N-Ethylformamide 73 C3H7NO 000627-45-2 9 4 Butane,* 2-methoxy-2-methyl- 102 C6H140 000994-05-8 9 Abundance Scan 264 (7.465 min): 31217.D (-) m/z 73.00 1 00.00% 73

5000 43 * ( 1 * i * * < * i , > ।**I**I*

103 7.20 7.40 7.60 7.80 T—! | I ! I I J I I I 1] I I I P ] l t I > TT 38 |, J 50 55, 60, 67,1 1,—B——87—OBBB0/0/B// m/z 43.001 " " miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573: 3-Pentanol, 3-methyl- 73

5000 7.20 7.40 7.60 7.80 55 m/z 45.00। 11.73% 45 87 27 39, 1 1 ‘‘ i ■ ■ ■ • i ■ ------- ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i 1 ■ ■ ■ i ■ ' ■ ■ i ■ ■

miz-> 10___ 20__ 30___ 40 50 60 70 80 90 100 110 Abundance 1/ s 73 n mr , । । .,। . n । ... i 7.20 7.40 7.60 7.80 5000 m/z 41;00 11.19% 45 15 53 59 88 ' ' I ' r' 1 i ■ ■ ■ ■ i ■ ■ ■ 1 i ■ ■ 1 • i ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ■ i ‘ ‘ ' i ■ ' ' ■ i ■ ■ ' ‘ i ■

m/z-> 10 20 30 40 50___ 60 70 80 90 100 110 Abundance #292: N-Ethylformamide T PFTrr 141 111 30 7.20 7.40 7.60 7.80 73 m/z 71.00 6.76% 5000 44 58

m/z-> 10 35. H 20 30 ' 1 I1 40 • i • • 50 60 i ■ • ■ ■ i

70 ■ 1 • ■ i

80 ■ ■ ■ • i

90 ■ ■ ■ 1

100 i 1 ■ ■ ■

110 i ' * ‘ 7.20 ‘ ' • • I 7.40 •+1*1* 7.60 7.80

31217.D GCMS0103.M Wed Feb 06 09:26:28 2002 Page 1

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