GCMS analysis results for sample AD29562, Jan 22 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\l\DATA\JAN0302\29562.D Vial: 21 Acq On 4 Jan 2002 6:02 am Operator: 209 GALOS Sample gems scan 1/2 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.46 4.39 ug/1 906413 1,4-Dichlorobenzene-d4 11.52

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 33 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 Silane, tetri methyl- 88 C4H12Si 000075-76-3 9 4 Pentane, 3-m thoxy- 102 C6H140 036839-67-5 9 Abundance 1 Scan 264 (7,465 min): 29562.D (-) m/z 73.00 100.00% I 73

5000 43 11,8,1 . i | 1 J !•' । •1 • । • | 7.20 7.40 7.60 7.80 i ■ 1 i ■ ■ • 1 I 1 1 1 1 I 1 , 38,141,50,55 1.i 1. ■. 67, I 103 • ■ f ■ + ■ i11 III-‘I1 87 m/z 43.0.5; 31.29% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573: 3-Pentanol, 3-methyl- 73 5000 7.20 7.40 7.60 7.80 55 m/z 45.05 11.65% 97 45 87 t _39 i Pi 1 II ‘ ----- miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide 30 73 —TmmgTTT I im-r r, . . , 7.20 7.40 7.60 7.80 5000 m/ Z 41.05; 10.82% 44 58 15 1118*1* miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62932: Silane, tetramethyl- I"4 kt"i r~ ri'| i it, । 11 TT" '( f 1′1 73 7.20 7.40 7.60 7.80 m/z 71.0.0 6.75% 5000

45 15 , 53 59 88____________ 1 ' I • ''' ‘ 1 1 1 1 1 1 1 1 1 1 I । । 1 ' i • • | । । i । । । + 1***14*111 1 । । t r । ■ > ■ j" * > । । . m/z~> 10 20 30 40 50 60 70 80 90 100 IIO 7.20 7.40 7.60 7.80

29562.D GCMS0103.M Fri Jan 11 08:33:58 2002 Page 1 NYC-WTC_000049877