GCMS analysis log for sample AD30696, Jan 2002

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Data File C: \HPCHEM\ 1 \DATA\DEC3101\30696.D vial: 33 Acq On 1 Jan 2002 7:57 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.

7.61 3.69 ug/1 943062 1,4-Dichlorobenzene-d4 11.67

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3 -Pentanol, 3 -methyl - 102 C6H140 000077-74-7 33 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 4 1-B anamine, 3 - methyl - 87 C5H13N 000107-85-7 7 Abundance Scan 280 (7.612 min): 30696.D (-) m/z 73.00 100.00% 73

5000 43 l * ‘ ‘ I ’ r 1 • I 1 ‘ ‘ I • ' 1 ' l ‘ '

87 7.20 7.40 7.60 7.80 8.00 _ , 1 50 55 60 67, । , I1.1. । । ■•■■■'■Y■ । ■ i'i1. ' ' ■ i ■ • ■i ■ ■ ■ ‘ i 103 ' ' m/z 43.00 31.49% miz-> 10 20 30 40। 50 60 70 80 90 100 110 Abundance #63573: 3-Pentanol, 3-methyl- 73

5000 —। । । . i । । । TV. . । . . 7.20 7.40 7.60 7.80 8.00 55 m/z 45.05 11.44% 27 45 87 1 39. 1 ■ ‘ i ‘ • ■ ■ . ■ ■ ■ ■ i ■ ■ ■ ■ i ■ ■ ■ • . ■ ■ *Bnnm ,.. -J.... miz-> 10 20 30 40 50 60 70 80 90 100 110

"Q Abundance #292: N-Ethylformamide 30 73 r r i PP, i'| ii TTTTTTTe 7.20 7.40 7.60 7.80 8.00 5000 m/ z 44 58

15 , ' J, . ! ! **I*0I**C* miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #82932: Silane, tetramethyl- PTPPmrmorTim i 1 1 73 7.20 7.40 7.60 7.80 8.00 m/z 71.00 6.56% 5000

45 15 I 53 59 I**** 111Bni ''''-'i'i . ■ • > t • II > • l • ■ • 88• TTr 1 ■ | i . . i | i Bmn—n—nmmpnT miz—> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80 8.00

30696.D GCMS1126.M Wed Jan 23 08:36:31 2002 Page 1

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