GCMS analysis log for sample AD30713, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC3101\30713.D vial: 28 Acq On 1 Jan 2002 3:07 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.62 3.91 ug/1 1118120 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3 -Pentanol, 3-methyl - 102 C6H140 000077-74-7 33 2 N-Ethyl formamide 73 C3H7NO 000627-45-2 9 3 Butane^z -methoxy-2-methyl- 102 C6H140 000994-05-8 9 4 Pentane, 3 -methoxy- 102 C6H140 036839-67-5 9 Abundance Scan 280 (7.618 min): 30713.D (-) m/z 72.95 100.00% 73

5000 43 - 7.20 7.40 7.60 7.80 8.00 miz-> ■ • i ■ • ‘ 10 । ■ ■ ■ ■ । ■ 20 30 38 |, | 50 55. .61 —— — 40 50 60 70 6744 , 80 87 * • • I ' ■ • i ■ • ■ ■ i 90 100 103 ‘ i • 1 110 m/z 43.00 32.32% Abundance #63573:3-Pentanol, 3-methyl- 73

5000 11nn————mTTTTT 7.20 7.40 7.60 7.80 8.00 55 m/z 41.00 11.28% 45 87 27 3?, I I 1**1111**s ■ । ■ • ■ । ■ ■ 1,1 rr 1 1 T1 1. . . m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide 30 73 =TpmmofTrre 7.20 7.40 7.60 7.80 8.00 5000 m/z 44.95 11.08% 44 58 15 • * • ■ t ■ • • • i • ■ • ‘ i ■ ■ ■ • i ■ ‘ I • ' 1 ' I ' ' ' 1 I ‘ ‘ ‘ ■ 1 1 1 miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1761: Butane, 2-methoxy-2-methyl- IBnnnn—nBBndmnnf 73 7.20 7.40 7.60 7.80 8.00 m/z 71.00 6.81% 5000 55 87 45 27 33 I • ■ i ■ • ■ 1 i ■ ■ ■ • i ■ • 1 ■ f • ■ ■ ■ i ■ 11 ‘i ""I1 Ter ■ ■ i ■ • ■ ■ । ■ ■' ■ । ■1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80 18 00

30713.D GCMS1126.M Wed Jan 23 08:46:17 2002 Page 1

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