GCMS comments for sample AD30484, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC3101\30484.D Vial: 8 Acq On : 31 Dec 2001 5:47 pm Operator: 209 GALOS Sample : gems scan 12/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.61 3.58 ug/1 881184 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 33 2 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 3 N-Ethylformamide 73 C3H7NO 000627-45-2 9 4 Butane,42-methoxy-2-methyl- 102 C6H140 000994-05-8 9 Abundance Scan 279 (7.609 mln): 30484.D (-) m/z 73.00 1 00.00% 73

5000 43 i ■ ■ ■ ‘ ■ 1 * ■ i ■ ■ ■ • i ' 11 I ' 1 381, | 50 55 6i 67, , 87 103 7.20 7.40 7.60 7.80 8.00 — > I 11** j 1 i i j r m/z 43.0, 31.77% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573: 3-Pentanol, 3-methyl- 73

5000 । T I I . । . I"T’I > > > I GT’ I I 7.20 7.40 7.60 7.80 8.00 55 m/z 45.05 11.59% 27 45 87

miz-> 9 > > । 1 1 1 1 i 1 1 1 • i'1 1 ' 1’go ■■ r • i'i । ) ■. < 10 20 30 40 50 60 ----- 70 80 90 100 110 Abundance #62932: Silane, tetramethyl- 73 7.20 ‘ 7.40 7.60 7.80 8.00 ' 5000 m/z 41.00 11.52% 45 15 | 53 59 88 > i V > > । j i t 4 i । I I J J J l i j » । >ii » "J T ‘I 1 1 11 I ' । » i • ■ ■ ‘ r ‘ » i i i m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide ’114*+1+’’’I 30 7.20 7.40 7.60 7.80 8.00 73 m/z 71.00 6.62% 5000 44 58

15 miz-> 1 ■ • i r-rr-r 1 r 1 ■ 1 I 1 ■ • ■ i ■ ■ 1 1 i ■ ■ • • i • t ■ ■ * • t •r‘ • i • ■ ■ • i *“■r • i”‘ • 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80 8.00

30484.D GCMS1126.M Wed Jan 16 08:26:17 2002 Page 1

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