GCMS analysis results for sample AD26320, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1401\26320.D Vial: 25 Acq On 16 Dec 2001 1:54 am Operator: 209 GALOS Sample : gems scan 12/10 a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.59 3.63 ug/1 893507 1,4-Dichlorobenzene-d4 11.67

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 33 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 Silane, tetramethyl - 88 C4H12Si 000075-76-3 9 4 1,3-Dioxolane, 2-methyl- 88 C4H802 000497-26-7 5 Abundance i Scan 278 (7.593 min): 26320.D (-) m/ z 73.00 100.00% 73

5000 43 87 7.20 7.40 7.60 7.80 8.00 ■ • । 38 1 50 55 ■ i > • • ■ i ■ • > > I • ■ ■ 1 1 ' 67, 1 ------- 1 ‘ । ■ ■ ■ ■ I 103 m/ z 43.00 27.64% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573: 3-Pentanol, 3-methyl- 73

5000 7.20 7.40 7.60 7.80 8.00 55 m/z 45.0.5 11.03% 45 87 27 l 39, 1 —P--——Bu———mTTT miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide 30 73 m —PIP ‘ 1rrr TTTT 7.20 7.40 7.60 7.80 8.00 5000 m/z 41.05 10.33% 44 58

15 — ——— mz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #845: Silane, tetramethyl- ---------- 73 7.20 7.40 7.60 7.80 8.00 m/z 71.00 6.77%

m/z-> 5000-

— ——— 10 15 20 -31 30 40 45 , I 50 55 1 ■ l ■ ■ ■ ■ I 60 70 ! I 80 88 ' ' ‘ ' i ■ 90 ’ 1 ' 1 1 1 1 1 i ' 1 100 110 7.20 7.40 1 7.60 7.80 8.00

26320.D GCMS1126.M Fri Dec 28 13:05:43 2001 Page 1

NYC-WTC_000037111