GCMS analysis results for sample AD30014, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC1801\30014.D Vial: 13 Acq On 19 Dec 2001 3:48 am Operator: 209 GALOS Sample : gc/ms scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.60 3.92 ug/1 1033140 1,4-Dichlorobenzene-d4 11.67

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3 methyl- 102 C6H140 000077-74-7 33 2 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 3 N-Ethylformamide 73 C3H7NO 000627-45-2 9 4 1,3 -Dioxolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 Abundance C Scan 278 (7.598 min): 30014.D (-) m/z- 73.00 100.00% 73

5000 43

87 103 7.20 7.40 7.60 7.80 8.00 67, । _8 I 50 55 i • ■ ' ■ i ' ■ ' ■ i ' ■ • ■ 1 1 1 • ' i • ,-i • ■ • ■ । -------- m/ z 43.00 28.41% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573: 3-Pentanol, 3-methyl- 73

5000 > I ' • ■ ■ I ■ — 7.20 7.40 7.60 7.80 8.00 55 m/z 41.00 10.61% 45 87 27 ■ ■ । ■ i • ■ • • । I , 39, 1 ■ ■ 'i' ■ ■ ■ । ■ ■ ''' । ■ ■ ■ ■ । ■ - । i < -

n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62932: Silane, tetramethyl- 73 I12r r TTuorr D TT T T PPTr TIT 7.20 7.40 7.60 7.80 8.00 5000 m/z 44.95 10.59% 45 ‘ 15 I 53 59 1 88 ■ 1 । ■ 'i ■ ■ । ' | • j ! > ' i-p-TTTTTTTTT-n m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide 30 7.20 7.40 7.60 7.80 .00 73 m/ z 71.00 6.35% 5000- 44 58

m/z-> 10 15 20 30 - 40 50 I ' ' ■ ' i ' ' ■ ' i ' ' • ■ i ' b ■ ■ i ■ ' ' ' i ' ' 60 70 80 90 100 110 ITT TT , , TT , 7.20 7.40 7.60 7.80 8.00

30014.D GCMS1126.M Tue Jan 15 15:36:03 2002 Page 1

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