DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2 701\30650.D Vial: 46 Acq On : 30 Dec 2001 3:26 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

7.62 2.68 ug/1 1240520 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3- hyl- 000077-74-7 33 102 C6H14O 2 Silane, tetramethyl- 000075-76-3 9 88 C4H12S1 3 N-Ethyl form; .ide 000627-45-2 9 73 C3H7NO _ 4 1,3 -Dioxolamne, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 Abundance Scan 280 (7.616 min): 30650.D (-) m/ z 73.00 1 00.00% 73

5000 43 7.20 7.40 7.60 7.80 8.00 ....................... 381 1 1 i 1 1 1 1 i 1 1 1 1 .............. . 1 J. 50,55, 60,67,1, , ‘ • i 1 1 87 i ■ ■ ■ ■ i 103 ' i ' m/ z 43.0.0 32.68% m/z-> 10 20 30 40 50 60 70 80 90 100 110 (Abundance #63573: 3-Pentanol, 3-methyl- 73

5000 7.20 7.40 7.60 7.80 8.00 55 m/z 45.05 11.74% 45 87 27 I , 39, 1 ■ 'i' ■ ■ ‘ ■ • 11 i 1 1 1 'i 1 ----- m/z—> 10 20 30 40 50 60 70 80 90 100 110 Abundance #52932 Silane ttraamethyl- 73

7.20 7.40 7.60 7.80 8.00 5000 m/z 41.00 10.60%

45 15 53 59 ............. 88............ ■ ■ i ' 1 ' ' i ■ 1 ■ ■ i ■ ' ' ■ i ■ ■ m/z-> 10 20 30 40 __ 50 60____ 70____ 80____90___ 100____ 110 Abundance #292: N-Ethylformamide T "11EI I I I I | 1 ! I 1 | I I I ! | I I

1 30 7.20 7.40 7.60 7.80 8.00 73 m/z 71.00 6.79% 5000 44 58

m/z-> ..15m 10 20 30 ' ' '40l" 11 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80 8.00

30650.D GCMS1126.M Mon Jan 28 11:18:02 2002 Page 1

NYC-WTC_000004371