GCMS analysis results, sample AD30022, January 2002

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Data File : C:\HPCHEM\l\DATA\DEC1901\30022.D Vial: 8 Acq On : 20 Dec 2001 6:18 am Operator: 209 GALOS Sample : gc/ms scan 12/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.60 3.79 ug/1 987490 1,4-Dichlorobenzene-d4 11.67

Hit# of .5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 33 2 1,3-Dioxolane, 2-methyl- 88 C4H8O2 000497-26-7 9 3 N-Ethylformamide 73 C3H7NO 000627-45-2 9 4 Pentane, 3-methoxy­ 102 C6H140 036839-67-5 9 Abundance/ Scan 279 (7.603 min): 30022.D (-) m/z 73.00 100.00% 73

5000 43 *0nn/23//m/mdm/bin 87 103 7.20 7.40 7.60 7.60 8.00 ... ..................... . 1 . | 50 5.5, 60 67, । 1+I**’I***1** ‘I1,1 1 r1'1 1 1 I 1 1 1 ' r‘ PI I**I*’’I* m/z 43.05 2 9.66% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573: 3-Pentanol, 3-methyl- 73 %

5000 7 20 ' 7.40 7.60 7.60 8.00 55 m/z 44.95 10.73% 45 87 27 | 39, 1 l ' ' ' ■'! ' J • • i • ■ 1111* m/z-> ■ ' i ' ■ ■ ‘ i • • • ‘ I1 ' • ■ i 1 ■ ■ ' i 1 • 10 20 30 40 50 60 70 80 90 100 110 Abundance #62902: 1,3-Dioxolane. 2-methyl- 73 *1unn—BmDnT ’ 18* 7.20 7.40 7.60 7.80 8.00 5000 43 m/z 41.0,0 10.33% 58 27 1 87 i. i ' 1 i ■ ■ ■ ■ i • ■ ■ • i 1 ' ' 1 i ' ■ • • i 1 < * i > 1 * • i * * * * । • > < * । > * i < । i < 1 ' i * m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide TTTTTPPPT 33 7.20 7.40 7.60 7.80 8.00 73 m/z 71.00 6.57% 5000 44 58

15 2m P ।i। ■ i • • ———————————— miz-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80 8.00

30022.D GCMS1126.M Wed Jan 02 16:05:03 2002 Page 1

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