GCMS analysis results for sample AD30353, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30353.D Vial: 17 Acq On : 28 Dec 2001 3:42 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.61 3.84 ug/1 1402320 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 33 2 1,3-Dioxolane, 2-methyl- 88 C4H802 000497-26-7 9 3 N-Ethylformamide 73 C3H7NO 000627-45-2 9 4 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 Abundance Scan 280 (7,613 min): 30353.D (-) m/z 73.0.0 100.00% 73

5000 43

m/z-> 38 |, | 50 55, $0 67, 1 —IT 87 7—i—|—i—J—i—!—j—C—i—j—।—i—j—i—11111 t11 r |11111 ' 1 * ।—i—i—I 11 * ।' i 10 20 30 40 50 60 70 80 103 1 i ■ ■ ■ ' I 1 1 ■ ' i ■ 90 100 110 m/z 7.4043 7.600 7.20 7.80 8.00 .90% Abundance #63573:3-Pentanol, 3-methyl- 73

5000 7.20 7.40 7.60 7.80 8.00 55 m/z 44.9,5 11.48% 45 87 27 I 39, | 1 1 i ■ ■ ■ ■ i 1 ■ ‘ ■ i‘ ■ ■ ■ i ■ • ■ ' i ■ 1 r' । ■ *'t ■ 1. 1 j m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62902 i 3-toxolane, 2-methyl 73

7.20 7.40 7.60 7.80 8.00 5000 43 m/z 41.0,0 10.98% 58 27 87 1 .___________ » • i ■ kit ‘1**1*+‘I‘ TL32 m/z--> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide **TTnnuuewnTprkemimm 30 7.20 7.40 7.60 7.80 8.00 73 m/z 71.0,0 6.53% 5000 44 58

15 m/z-> 0 10 20 30 ■ • I 40 ’ i • ■ 50 60 । ■ ■ ■ ■ । 1 1 ■ ■ i 1 ■ • • i ■ 1 ■ ■ i ■ 1 ■ ■ i ' 70 80 90 100 110 In . . . । 7.20 7.40 । . i । ■ jn-.-T] . . 7.60 7.80 8.00

30353.D GCMS1126.M wed Jan 02 10:52:35 2002 Page 1

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