GCMS analysis results for sample AD31463, Feb 11, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN1602\31463.D Vial: 22 Acq On : 17 Jan 2002 8:09 am Operator: 209 GALOS Sample : gc/ms scan 12/28 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 7.45 2.60 ug/1 646249 1,4-Dichlorobenzene-d4 11.50 Hit# of 5 Tentative ID MW MolForm CAS# Qual

l 3-Pentanol, /-methyl- 102 C6H140 000077-74-7 33 2 Silane, tetramethyl- 88 C4H12Si 000075-76-3 25 3 N-Ethylformamide 73 C3H7NO 000627-45-2 9 4 1,3-Dioxolane, 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 Abundance Scan 262 (7.446 min): 31463.D (-) m/z 73.00 100.00% 73

5000 43

7.20 7.40 7.60 7.80 -ppmpep .. 11139, J 50 55.60 67,1 . 87 103 '•‘-• I ri ' ■ ■ ' I >’■ • ' i ■ ' m/z 43.05 33.15% mz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573:3-Pentanol, 3-methyl- 73

5000 1111*11-44*, 411 • i • • 7.20 7.40 7.60 7.80 55 m/z 45.05 11.77% 45 87 27 I , 39, ■ । • ■ : ■ ■ i 1 ■ TTum 1 i ■ I ■ ■ i ■ ■ ’j ' i ■ ■ ■ 1 I 1 ' 1 ' i ‘ 1 m/z->10 20 30 40 50 60 70 80 90 100 110 Abundance e S2te. retramethyi 73 - r. . , । r t-> । |'i । i i /tt ITTi 7.20 7.40 7.60 7.80 5000 m/z 41.00 11.62% 45 15 53 59 ■ ■ i ■ ■ • 1 i • ■ 1 ■ i 1 • ■ 1 i 1 ■ ■ ■ i • ■ ■ • i ‘ 88 ■ i ' ■ ■ ■ i ■ r r 1 I 1 1 1 1 I 1 ' 1 1 I 1 1 rn/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide TTTTTmmerro 30 7.20 7.40 7.60 7.80 73 m/z 71.00 6.38% 5000 44 58

15 ---PI- ST 1*1111 . i > I rt. . I . . . : (kin i I | I I miz-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80

31463.D GCMS0103.M Thu Feb 07 12:40:38 2002 Page 1

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