GCMS analysis summary, sample AD31378, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\J2ySF1502\31378.D Vial: 13 Acq On : 15 Jan 2002 10:42 pm Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.45 4.64 ug/1 1120430 1,4-Dichlorobenzene-d4 11.50

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 33 2 1,3-Dioxplane, 2-methyl- 88 C4H802 000497-26-7 9 3 N-Ethylformamide 73 C3H7NO 000627-45-2 9 4 Silane/ tetramethyl- 88 C4H12Si _____ 000075-76-3 9 Abundance T Scan 262 (7.453 min):31378.D (-) m/z 73.00 100.00% 73

5000 43

, 87 103 7.20 7.40 7.60 7.80 38 |, | 50—55, --111/1///1/n//11//1 60 67, । ' ■ ■ i 1 ■ nr//*nnIr i ■ 1 ■ ■ i ■ '■ ■ ■ i ■ 1 m/z 43.00 31.64% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63572:3-Pentanol, 3-methyl- 73

5000 1 *1 • ।1 ■,i !■ ■ ■ ■ ।1•।■

55 7.20 7.40 7.60 7.80 45 87 m/z 45.05 11.80% 27 m/z-> 10 C 20 30 40 50 —1 ■ ■ i ■ ■ • • i • ' ■ • i • ■ ■ • i ■ ‘ 60 70 80 90 100 110 Abundance 482002 1,3-otpiane 73 ■ ■ r11 ‘ ‘ ■ i 1 ■ i ■ ■ .7.20 7.40 7.60 7.80 5000 43 m/ z 41.05 10.81% 58 27 87 i ' 1 I 1 ' ' 1 I ' ' "I’ 11 INU"ATTTTTT1t | I I I I | I I I ■ I | 1 T ■ • । ■ i • 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide 7.20 7.40 7.60 7.80 73 m/ z 71.00 6.58% 5000 44 58

15 010 ' 1 Alat r1 i 1 • I ' 1 ■ i ■ 1 • ' i 1 1 ■ 1 1 1 ‘ ' i ■ ■ ' ■ i ' 1 ( ■ i ■ ■ ■ i ■ ■ ■ ■ i • • ’ • i * • miz-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80

31378.D GCMS1126.M Mon Feb 04 15:25:56 2002 Page 1

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