GCMS analysis results for sample AD31364, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\JAN1602\31364.D Vial: 16 Acq On : 17 Jan 2002 2:18 am Operator: 209 GALOS Sample : gc/ms scan 12/27 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.44 3.99 ug/1 1019890 1,4-Dichlorobenzene-d4 11.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 33 2 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 4 Pentane, 3-methoxy-__ 102 C6H140 036839-67-5 9 Abundance ' Scan 261 (7.443 min): 31364.D(-) m/z 73.00 100.00% ! 73

5000 43 I******1**’I । TTt r | i <■ 7.00 7.20 7.40 7.60 7.80 36 , 50 55, 60 67, , , 87 94 103 0- —11————————— 1 ■ i r "j । । ’ i t । i i « > । । । t i । i rn/z 43.00 33.62% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573:3-Pentanol, 3-methyl- 73

5000

27 I 39, 1 .. 45 . ! 55 ; 87 m/z "TT 7:00 7.20 7.40" 7.60 7.80

■ ' i ■ ■ ■ ‘ i ■ ■ ■ ' i ■ 1 • ■ i • ■ ■ ■ i ■ 1 ‘ • i ■ ■ ■ ■ i • 1 ■ 1 i ■ ■ ■ ' i ■ • ■ 1 i • • ■ ■ i ■ miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance 763 1-dfanpti snofhyle 30 -TTmpT 7.00 7.20 7.40 7.60 7.80 5000 m/z 41.0,5 11.95%

15 41 55 70 87 11dn/mmT—*1u—**11/*211—*7_**01*—1‘9—Ir miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #845: Silane, tetramethyl- "RpTrgdmgmopuir 73 7.00 7.20 7.40 7.60 7.80 m/z 71.00 6.71% 5000

45 15 31 88 ‘ 1 i ‘ ‘ ‘ ‘ I ‘ 1 ’ • T*r ------- ■ ■ i 1 ■ ' 1 I ■ ■ ■ ■ I ■ • • > I 1 I . . 1 . [+8/8/8 | . I I J | J n 1114 m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.00 7.20 7.40 7.60 7.80

31364.D GCMS0103.M Thu Feb 07 09:12:19 2002 Page 1

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