GCMS sample analysis report, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\JAN1802\31552.D Vial: 15 Acq On : 19 Jan 2002 5:15 am Operator: 209 GALOS Sample : gc/ms scan 12/31 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.44 4.06 ug/1 1003790 1,4-Dichlorobenzene-d4 11.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3/methyl- 102 C6H140 000077-74-7 33 2 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 3 Butane, 2-methoxy-2-methyl- 102 C6H140 000994-05-8 9 4 Silane, tetramethyl- 88 C4H12S1 000075-76-3 9 Abundance Scan 261 (7.444 min): 31552.D (-) m/z 73.00 100.00% 73

5000 43 1 ‘ • 1 i ■ ■ ' ■ i ■ ■ ■ ■ i ‘ 1 i • 1 ■

87 103 7.20 7.40 7.60 7.80 0- ............................ 38.1,1.1 50.55 60 67, । , TRTnn/nb m/z 43.0,0 32.45% ' 1 1 1 1 1 1 1 1 1 1 ' i ■ ■ 1 1 I1 1 ‘ 1 । 1 ' I 1 s’s’i 14*1*11** m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573:3-Pentanol, 3-methyl- 73

5000 7.20 7.40 7.60 7.80 55 m/z 45.05 12.13% 45 87 27 ‘ 1 1 1 11 1 1 1 i ■ ■ । ■ , 39, j ■i' ■ ■ ' i 1 r' । 1 ''i ■ ' ■ ■ i ■ ■ 1 ' i ' ‘ ' i ■ ■ ' ■ i ■ ' m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #763: 1 -Butanamine _ -methyl- 30 .................. ' ‘ I ' l1 ‘ ‘ ■ I ' 1 ' ' I ‘ I ‘ ‘ ' 7.20 7.40 7.60 7.80 5000 m/z 41.0.0 11.64%

15 41 55 70 87 • ‘ i ■ ' ‘ ‘ i ' • 1 ■ i 1 1 ■ ■ i ■ ‘ ■ ■ I ' ■ ■ • i ' ' ■ ■ i ■ ' ■ • i ■ • ‘ • i 1 ■ • ‘ i ‘ 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1761: Butane, 2-methoxy-2-methyl- — i . . i 144* I 4 » i » | । 1117t rrr 73 7.20 7.40 7.60 7.80 m/z __ 71.00 7.17% 5000 55 87 45 ■ • । 27 33 1 • i ■ • > < l < > ■ • । • • > ■ । • • 1 ■ । *’1* —Pmm ■ ■ i 1 1 miz-> 10 20 30 40 50 60 70 80 90 100 110 ' ‘ ' 7.20 " 7.40 ' 7.60' ' 7.80

31552.D GCMS0103.M Wed Feb 06 15:42:36 2002 Page 1

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