GCMS analysis results for sample AE00010, Feb 13 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN2402\10.D Vial: 13 Acq On : 25 Jan 2002 12:50 am Operator: 209 GALOS Sample : GC/MS SCAN 1/3 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.43 3.43 ug/1 993102 1,4-Dichlorobenzene-d4 11.48

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol/ 3-methyl- 102 C6H140 000077-74-7 36 2 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 4 Pentane, 6-methoxy-_________________ 102 C6H140 036839-67-5 9 Abundance Scan 260 (7.434 min): 10.D (-) m/ z 73.00 1 00.00% 73

5000- 43 I 1 1 1 1 I 1 1 1 1 1 1 1 1 7.00 7.20 7.40 7.60 7.80 i ' 1 1 ■ i ■ ■ ■ • i 38■ I 1,' 1 1 ■ 1 501 551 1 i • ■ 67, I ■ '!■ |.. 7 103 , m/ z 43.05 33.19% m/z-> 10 20 30 40 50 60 70 80 90 100 110 ’Abundance #63572: 3-Pentanol, 3-methyl- I 73

5000- 55 7.00 7.20 7.40 7.60 7.80 45 87 m/z 45.05 12.27% 27, । • ■ • ■ । ■ ■ ■ • । , ! ■ 11 • • > । > ■ । ■ । 1 . _ i ■ ■ ' ' i I, m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #763: 1-Butanamine. 3-methyl- 30 i ' ■ ' 1 i ' —P • /On ■'i 1 1 • 7.00 7.20 7.40 7.60 7.80 5000- m/ z 41.05 11.50%

15 j____ 41 55 70 87 ■ ■ TO ■ I ' ' ■ ■ i ' ' i 1 ' 1 ' i ' ' i ' ' ■ ' I ' ' ' ' i ' ' ' ' i ' ' ' ' i ' ' ' ‘ i ' ' miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #845: Silane, tetramethyl- PPT • । । । > । 73 7.00 7.20 7.40 7.60 7.80 m/Z 71.00 6.92% 5000

45’ 15 31 , .1 —II———mmTTTTTTTT 55 ..... 88.......... m/z--> 10 20 30 40 50 60 70 80 90 100 110 7.00 7.20 7.40 7.60 7.80

10.D GCMS0208.M Fri Feb 08 13:36:22 2002 Page 1

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