GCMS analysis results for sample AD30252, Jan 2002

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Data File : C:\HPCHEM\1\DATA\DEC2701\30252.D vial: 22 Acq On : 28 Dec 2001 9:31 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

7.61 4.00 ug/1 1333510 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 33 2 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 3 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 4 Pentane, 3-methoxy- 102 C6H14O 036839-67-5 9 Abundance Scan 280 (7.611 min): 30252.D (-) m/z 72.95 100.00% 73

5000 43 7.20 7.40 7.60 7.80 8.00 ■ ■ i ■ ‘ ■ i • ' 1 ' i ' , 38,1,,1 50 55.60 , 87 103 1‘r 1 1 s’i’d" ■ ■ 67+4 I ■ ■ l ■ 1*111 । । । । । । ■■> i i । । m/z 43.00 31.36% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63573: 3-Pentanol, 3-methyl- 73

5000 TTunnBmB 1 i 1 ■ 7.40 7.60 7.80 8.00 7.20 45 55 87 m/z 45.0,5 12.18% 27 • • i • • ■ ‘ i ■ ■ • ■ i‘ ' ■ ' i 1 • ‘ 1 39, 1 । 1 1 r‘ । ■ ■ । 1 1 ■ ■ i • ■ ■ ■ 1*+*’I* m/z-> 10 20 30 40 60 50 70 80 90 100 110 Abundance #62932: Siiane, tetramethyl- 73 TTuT ■ i ■ ■ ‘ । ■1 1 ■ i ■ 1 7.207.40 7.60 7.80 8.00 5000 m/z 41.0,5 11.48%

45 15 53 59 88 ■ ■ i ■ ■ ■ ‘ i 1 ■ ■ ■ i • • • ■ i ■ ■ ■ ' i ' ' i ■ ' 1 ■ i ' ‘ ■ i 1 miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #763: 1-Butanamine, 3-methyl- =TTTTTu*)1 1 1 1 1 1 1 i 35 7.20 7.40 7.60 7.80 8.00 m/z 71.0.0 6.49% 5000

miz-> ■ ■ i ' 10 15 1 i • ■ 20 30 41 ■ । -Ti 1 40 50 55 60 70 70 80 87 90 100 110 7.20 m 7.40 7.60 7.80 8.00

30252.D GCMS1126.M Wed Jan 02 10:42:05 2002 Page 1

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