GCMS analysis summary, sample AD31374, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN1502\31374 .D Vial: 19 Acq On : 16 Jan 2002 4:34 am Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.45 4.05 ug/1 962621 1,4-Dichlorobenzene-d4 11,50

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H14O 000077-74-7 33 2 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 3 Pentane, 3 -methoxy- 102 C6H140 036839-67-5 9 4 Silane, tetramethyl - 88 C4H12Si 000075-76-3 9 Abundance i? Scan 262 (7.446 min): 31374.D (-) m/z 73.00 100.00% 73

5000 43 ■ ■ । ‘ । ■ i • 1, ■ ■

87 103 7.20 7.40 7.60 7.80 --3850556674 '' ’ 1 i 1 1''11 i 1 ' 1 1 1 1'1 1 1 i 1 m/z 43.00 32.59% miz-> 10 20 30 40 50 60__ 70 80 90 100 110 Abundance #63573:3-Pentanol, 3-methyl- 73

5000 • ■ ■ ■ i ■ ■ 1 ■ i ■ ■ ‘ • i ■ ‘ ' * , . * . 7.20 7.40 7.60 7.80 55 m/z 45.0,0 12.39% 45 87 27 1 3.9, 1 1*nnmnn/n—//=*/m/B1/nBaon I * > । < । । । . miz->__ 10 __ 20 30 40 50 60 70___ 80___ 90___ 100 110 Abundance 6 -narine 3-mafryi- 30

7.20 7.40 7.60 7.80 5000 m/z 41.00 11.59%

15 41 55 70 87 i ■ ■ ■ ■ i ■ ■ ' ■ i ■ ■ ■ ■ i ■ 1 ‘ ‘ i ■ ■ ■ • i ■ ■ • • , ■ ■ • 1 i ■ ■ ' ' i 1 1 ■ ‘ i 1 ■ • ■ i ■ m/z-> 10 20 30 40 50 60 70 80 90___ 100 110 Abundance #1793: Pentane, 3-methoxy- 73 7.20 7.40 7.60 7.80 m/z 71.0,0 6.90% 5000 45

. .33 39, ’ ‘ 1 ‘ ‘ ‘ I ‘ 4 1 ‘ I ‘ ‘ ‘ ‘ I1 ‘ ‘ 55 0 11 I’1 ‘t/nnIO/TTTnuon m&~> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80

31374.D GCMS1126.M Mon Feb 04 15:05:03 2002 Page 1

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