GCMS analysis summary, sample AD31374, Feb 2002

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Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\JAN1502\31374.D Vial: 19 Acq On : 16 Jan 2002 4:34 am Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.14 0.34 ug/1 101026 Naphthalene-d8 15.09

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopent asiloxa: , decamethyl - 370 C10H3005Si5 000541-02-6 64 2 3,4 - D i hydroxyben yl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 32 3 N-(Trifluoroacetyl)-0,0',0''-tris(t 481 C19H34F3NO4Si3 000000-00-0 28 4 Benzoic acid, 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 25 Abundance Scan 991 (14.139 min): 31374.D (-) 73 m/z 73.00 100.00%

5000 267 355 45 —— 108 133154 I?3 223 , ; 323 13.80 14.00 14.20 14.40 ‘ ‘ ‘ —1— r i 1 A m/z 267.00 29.01% m/z~> 50 100 150 200 250 300 350 400 450 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 13.80 14.00 14.20 14.40 m/z 355.0 20.10% 1, 207 .1 323 | ' i ■ ' ‘ ‘ I 1 miz-> SO' ' ' 100 ' ’ 150 ‘ ' 200 250 300 350 400 450 Abundance #a 8E8: 2 Dihvmyybenz alouhdrisemgmgmyis 73

13.80 14.00 14.20 1440 ‘'1 267 m/z 44.95 7.73% 5000 179 356 . 45 147 ' I ■ • i ■ ' • ■ i ' i 209 237 J 312 .............. m/z-> 50 100 150 200 250 300 350 400 450 Abundance #58326: N-(Trifluoroacetyl)-O,O',O"-tris(trimethylsilyl)no 73 13.80 14.00 14.20 1440 ‘ ' 355 m/z 267.90 7.67% 5000

45 1, 126147 193 265 1 376 481 ■ i 1 m/z-> 50 100 150 200 250 300 350 400 450 13.80 14.00 14.20 14.40

31374.D GCMS1126.M Mon Feb 04 15:05:08 2002 Page 2

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