DEP GCMS data table, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC2701\30641.D Vial: 42 Acq On : 29 Dec 2001 11:33 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

14.31 2.06 ug/1 1100520 Naphthalene-d8 15.28

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 74 2 3,4-Dihyd: xybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 38 3 N- (Triflu roacetyl)-0,0',0''-tris(t 481 C19H34F3NO4Si3 000000-00-0 37 4 Benzoic /acid, 2, 5-bis (trimethyl silo 370C16H3004Si3 003618-20-0 37 Abundance Scan 1009 (14.309 min): 30641.D (-) m/ z 73.00 100.00% 73

5000 267 355 14.00 14.20 14.40 14.60 ! i 0- TI 45 , 108 133154 , ,193223 247 293 323 L........... m/z 267.00 36.91% miz-> 50 100 150 200 250 300 350 400 450 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 14.00 14.20 14.40 14.60 m/ z 355.05 28.61% ........... 207 323 1 ■ i m/z-> 50 100 150 200 250 300 350 400 450 Abundance #10858. 3.4-Diydroxybenzya alcohol,tris(trimethtyislly}- 73 14.00 14.20 14.40 14.60 267 m/z 356.05 10.10% 5000 179 356 45 147 ............ 209 237 i 312 ....................................... I m/z-> 50 100 150 _ 200 250 300 350 400___ 450 Abundance #58326: N-(Trifluoroacetyl)-b,O',O'’-tris(trimethylsiiyljno 7b 14.00 14.20 14.40 14.60 355 m/z 267.90 9.35% 5000

45

m/z-> 50 h—100 126147 150 11 ‘i 1 ■ ■ 193 ■ 200 i ■ ' ■ ■ 250 i 265 ■'' 300 350 376 400 450 481 14.00 14.20 14.40 14.60

30641.D GCMS1126.M Mon Jan 28 11:13:47 2002 Page 2

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