GC/MS calibration data for sample 30647, Dec 2001

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Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018546–000018575

Folder label: “GCMS X 12/18/01 A 12/30/01”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2 701\30706.D Vial: 54 Acq On : 30 Dec 2001 12:10 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

14.31 3.44 ug/1 1794230 Naphthalene-d8 15.28

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane , decamethyl - 370 C10H3005Si5 000541-02-6 64 2 3,4-Dihydr< benzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 43 3 N-(Trifluoroacetyl)-0,0’,0”-tris(t 481 C19H34F3NO4Si3 000000-00-0 43 4 Benzoic acid, 2-[(trimethylsilyl)ox 282 C13H2203Si2 003789-85-3 38 Abundance Scan 1009 (14.305 mln): 30706.D (-) m/z 73.00 100.00% 73

5000 267 355 .7 45 14.00 14.20 14.40 14.60

miz-> I i • • i ’ ■ 50 108133154 193 223 247 4 293 323 —————— 100 150 200 250 300 350 —4 • I 1 1 1 1 I 400 450 ' m/z 267.00 33.77% Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 T T T 1 14.00 14.20 14.40 14.60 m/z 355.05 24.96% , ...... 207 • • , I 323 , l ' 1 i •" • ■ i ■ • ' ■

m/z—> 50 100 ' 150 200 250 300 350 400 450 Abundance #49868; 3,4-Dinydroxybenzyl alcohol, tris(trimethylsilyl)- 73

14.00 14.20 14.40 14.60 267 m/z 267.90 9.00% 5000 179 356 45 147 1 209 237 , 312 ...... ...... T ‘ I • ' ■ • I-‘ ‘' T11L r1IT miz-> 50 100 150 200 250 300 350 400 450 Abundance #58326: N-(Trifluoroacetyl)-O,O',O"-tris(trimethylsilyl)no 73 14.00 14.20 14.40 14.60 355 m/z 356.0 8.98% 5000

45 I l, 126147 193 265 376 481 ■ ■ i ■ ■ ‘ ' I-1*—■ I ‘ ' ' 111—1rdrtnr ■ ■ ' ’' i ■ ■ i “ > 1 r> • » ■ ti । n n । > > i r । i i i i । i i i i । miz-> 50 100 150 200 250 300 350 400 450 14.00 14.20 14.40 14.60

30706.D GCMS1126.M Fri Feb 01 11:08:00 2002 Page 3

NYC-WTC_000018563

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