GC/MS calibration data for sample 30647, Dec 2001

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Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.

NYC-WTC_000018546–000018575

Folder label: “GCMS X 12/18/01 A 12/30/01”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\DEC2701\30706.D Vial: 54 Acq On : 30 Dec 2001 12:10 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

11.13 1.20 ug/1 498088 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclotetr; iloxane, octamethyl- 296 C8H24O4S14 000556-67-2 83 2 2-Oxo-4^ enyl-6-(4-chlorophenyl)-1 282 C16H11C1N2O 000000-00-0 9 3 6,7-Benizo-phenothiazine-5, 5-dioxide 281 C16H11NO2S 000000-00-0 9 4 Benzene, 1-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 9 Abundance ′ Scan 663 (11.129 min): 30706.D (-) .................. rn/z 281.00 100.00% 281

5000 ’ ‘ I ‘ ‘ ‘ I * r • ' I • * ‘ ‘ I 10.80 11.00 11.20 11.40 .45 59 7 ,87,,103,11923147 163 177 12,297 221,235 J'9,265 I. m/z 282.00 29.57% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 (Abundance #41966: Cyclotetrasiloxane, octamethyl- 281

_________ / 5000 • • i ■ ’ • • i • * • • i • ’ k * i 10.80 11.00 11.20 11.40 m/z 283.00 18.18%

m/z-> 40 60 3395| 80 100 120 140 160 180 200 220 240 260 280 Abundance #39756: 2-Oxo-4-phenyl-6-(4-chloropheny)-1 2-dihydropyrimi 281 T "int ‘ ‘ • i 10.80 11.00 11.20 11.40 5000 m/z 192.9,0 13.46%

102 123 141 175 204 247 - m/z-> 40 60 " 80 100 120 140 160 180 200 220 240 260 280 Abundance #39602:6,7-Benzo-phenothiazine-5,5-dloxide 19 — I‘‘‘I 281 10.80 11.00 11.20 11.40 m/z 73.00 10.84% 5000 217 232

m/z-> ’ • I ‘ *+4252264 102 118 ‘ ‘ J * ‘ ‘ 1 1 ’ ‘ ’ 1 1 1 ’ ‘ ‘ t ‘ ‘ ‘ ‘ I • • * • I ‘ ‘ 40 60 80 100 120 140 160 180 200 220 240 260 280 ‘ I ‘ 189 204 li T-r-p-r p 11111 10.80 11.00 11.20 11.40

30706.D GCMS1126.M Fri Feb 01 11:07:55 2002 Page 2

NYC-WTC_000018562

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