Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
NYC-WTC_000036162–000036183Folder label: “GCMS X 12/3/01 A 12/10/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC27O1\29231 .D Vial:•57 Acq On : 30 Dec 2001 3:05 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/18 A Inst : GC/MS 2 09 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K. L ********************************************************************* Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 6
R.T. EstConc Area Relative to ISTD R.T.
11.13 1.05 ug/1 1111090 1,4-Dichlorobenzene-d4 11.68
Hit# of 5 ntative ID MW MolForm CAS# Qual
1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 86 2 2-Oxo-4-phenyl-6- (4-chlorophenyl)-1 282 C16H11C1N2O 000000-00-0 9 3 6, 7-Benzo-phenothiazine-5, 5-dioxide 281 C16H11NO2S 000000-00-0 9 4 Benzene, 1-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 9 Abundance Scan 663 (11.128 min): 29231.D (-) m/z 281.00 100.00% 281 I
5000- —............ 193 207 45 59 ‘3 85 103 119 133 | 147 163 179 J 249 265 10.80 11.00 11.20 11.40 1P—mT TT’P—naumnTT - 221 235 L — m/ z 2 82.00 28.75% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #41966: Cyclotetrasiloxane, octamethyl- 281
5000 10.80 11.00 11.20 11.40 m/ z 2 83.00 17.44% 73 133 163 177 191 101 207 | 235 249 265 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39756: 2-Oxo-4-phenyl-6-(4-chlorophenyl)-1,2-dit)ydropyrirni 281
10.80 11.00 11.20 11.40 5000- m/z 192.90 12.42% I h ................. 102 123 ......... 175 , ........ 247 ..... .. miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39602: 6,7-Benzo-phenothiazine-5,5-dioxide / i 281 10.80 11.00 11.20 11.40 m/z 133.00 11.67% 5000- 217 232 102 118 189 204 l|.i 252264 • 1 l > • 1 • l > • • ■ l > ■ m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 10.80 11.00 11.20 11.40
29231.D GCMS1126.M Mon Dec 31 13:59:11 2001 Page 2
NYC-WTC_000036169
OCR can misread numbers and units. Confirm readings against the page image before using them.
Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.
No available related records indexed in this group.
NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018470
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018492
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017748
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018519
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017833
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017808
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017724
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
Page similarity is temporarily unavailable or this page has no indexed vector.
Readers open these alongside this record — through an Ask answer, the same folder, or indexed similarity. Not a claim they are about the same event.
NYC-WTC_000036040
Department of Environmental Protection record logging GCMS X samples from November to December 2001.
Filed in the same folder
NYC-WTC_000036041
Fragmented document page from DEP Box 22 containing partial text regarding GCMS procedures or logs.
Filed in the same folder
NYC-WTC_000036044
Technical form recording method parameters, drip rates, and analytical data for GCMS testing procedures.
Filed in the same folder
NYC-WTC_000036055
Laboratory report listing detection limits for various organic compounds in a GCMS blank sample run on December 18.
Filed in the same folder
NYC-WTC_000036059
Calibration report detailing response factors for standard compounds used in GCMS analysis of sample AD29135.
Filed in the same folder