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GCMS analysis results for sample AD29563, Jan 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.

NYC-WTC_000036712–000036728

Folder label: “GCMS X 12/7/01 A 1/2/02

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Scanned page image, NYC-WTC_000036720
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NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\HPCHEM\1\DATA\DEC2701\29563.D Vial: 36 Acq On : 28 Dec 2001 11:11 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/7 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclotetrasiloxane, octamethyl Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

11.13 0.83 ug/1 352887 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentative I MW MolForm CAS# Qual

1 Cyclotetrasiloxane, octamethyl- 296 C8H24O4Si4 000556-67-2 83 2 2-Oxo-4-phenyl-6-(4-chlorophenyl)-1 282 C16H11C1N2O 000000-00-0 9 3 6, 7-Benzo-phenothiazine-5,5-dioxide 281 C16H11NO2S 000000-00-0 9 4 Benzene, l-phenyl-4-(2-cyano-2-phen 281 C21H15N 027869-56-3 9 Abundance ' Z Scan 663 (11.128 min): 29563.D (-) m/z 281.00 100.00% 281

5000 i 1 ‘ ■ i ■ ' ' ■ i 73 133 193 249 265 10.80 11.00 11.20 11.40 45 59 | 89 103 119 1147 163 177 ll, 207 221 235 I, |„ — 11 1 1 11 1 1 r rr m/z 282.00 29.25% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 'Abundance #41966: Cyclotetrasiloxane, octamethyl- 281

5000 - _10.80 11.00 11.20 11.40 207 m/z. 283.00 17.69% 73 133 235 249 265 | I 163 177 191 -X ■ ' i • ■ ■ ■ i ■ ■ ‘ ■ i ' ■ ■ ■ i m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #39756: 2-Oxo-4-phenyl-6-(4-chloropheny!)-1,2-dihydropyrimi 281 10.80 11.00 11.20 11.40 5000 m/ z 192.90 11.72%

102 123 141 175 204 47 m/z--> 40 60 80 100 120 140 160 180 200 220 240 260, 280 Abundance #39602: 6,7-Benzo-phenothiazine-5,5-dioxide - ----- 281 10.80 11.00 11.20 11.40 m/ z 73.0.0 10.43% 5000

217 232 . 102 118 129.20444 ,, ii,| r +252264 — ■ ■ 17 ■ r i । , . , , । m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 10.80 11.00 11.20 11.40

29563.D GCMS1126.M Tue Jan 08 11:42:11 2002 Page 2

NYC-WTC_000036720

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NYC-WTC_000036720Source: NYC Law Department, mirrored locally

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