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GCMS analysis results for sample AD29563, Jan 2002

Machine-extracted title · confidence 100%

GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.

NYC-WTC_000036712–000036728

Folder label: “GCMS X 12/7/01 A 1/2/02”

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Scanned page image, NYC-WTC_000036719
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NYC 9/11 Public Portal Document

Library Search Compound Report

. Data File : C:\HPCHEM\l\DATA\DEC2701\29563.D Vial: 36 Acq On : 28 Dec 2001 11:11 pm Operator: 209 GALOS Sample : GC/MS SCAN 12/7 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 1-Butanamine, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.61 3.02 ug/1 1278560 1,4-Dichlorobenzene-d4 11.68

Hit# of 5 Tentati ID MW MolForm CAS# Qual

1 1-Butanamine, 3-methyl- 87 C5H13N 000107-85.-7 9 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 4 Pentane, 3-methoxy- 102 C6H140 036839-67-5 9 Abundance 7 Scan 280 (7.612 min): 29563.D(-) m/z 73.00 100.00% 73

5000- 43 i • ■ ■ ■ i ■ ■ 7.20 7.40 7.60 7.80 8.00 m/z-> 0 p n q ft r. | , TpmggilR4 87 103 j 1 1'• (‘ 1'' |’1 1 ' i‘ 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 'I ' '’ ‘ I‘ ’I ‘ 208 ‘I ' m/ z 43.0,5 32.61% [Abundance #763: 1-Butanamine, 3-methyl- 30

5000 7.20 7.40 7.60 7.80 8.00 m/z 45.05 11.57% 15 TTUT.... I 41 55 70 | , M | I I M | 87 | . I I | . . M | , M , | , H i | l ! < ! | < f, I | I I I I | I | I | | | | | i■ ■i m/z--> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #292: N-Ethylformamide 3'0 73 1 r1 ■ 1 1 । ■ 7.20 7.40 7.60 7.80 8.00 5000- m/ z 41.0.5 11.25% 44 58

15 ! i T’TDUTTTTTTTTTCTUTTTUTTTTTTTTTTTTTTTWTTTTUTTTTTTTTT ' ’ I" ’ 'I” T‘ TTTTT‘T‘ m/z--> 10 20 30 40 50 60 70 80 90 100110120130140150160170180190200210 Abundance #62932: Silane, tetramethyl- 73 7.20 7.40 7.60 7.80 8.00 m/ z 71.00 6.99% 5000-

45 15 | 55 i •"' HHmT 1 88 EI—UEITT’ in, | « . I I | . I I . | TT < | . I . I | | | I I | I I I 1 1 1 1 1 1 1 1 ......................... m/z-> 10 20 30 40 50 60 70 80 90 100110 120130 140 150160 170180190 200 210 7.20 7.40 7.60 7.80 8.00

29563.D GCMS1126.M Tue Jan 08 11:42:06 2002 Page 1

NYC-WTC_000036719

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NYC-WTC_000036719Source: NYC Law Department, mirrored locally

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Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

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