GCMS analysis results for sample AE01442, Mar 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB2102\1442 .D Vial: 14 Acq On : 22 Feb 2002 2:54 am Operator: Sample : gc/ms scan 1/22 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 1-Butanamine, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.20 0.36 ug/1 25531 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual A _____ 1 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 2 1-Butanamine, 2-methyl- 87 C5H13N 000096-15-1 7 3 N-Ethylformamide 73 C3H7NO 000627-45-2 5 4 Formamide/ N,N-dimethyl- 73 C3H7NO 000068-12-2 5 Abundance / Scan 344 (8.203 min):1442.D (-) m/ z 73 700.... 100.00% 73

5000 43 ‘ i ' ■ ■ ■ i ■ ' ■ ' i ■ ■ 8.00 8.20 8.40 8.60 7.80 m/z-> -HH 51 55 TTTTTT 1.. ft1,?/... m/z 43.05 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 69. 29.00% Abundance #763: 1-Butanamine, 3-methyi- 30 ........................ ...

5000 7.80 8.00 8.20 8.40 8.60 m/z 44.95 11.30% 15 27 4144 55 58 70 87 WTRWP11POTT m/z-2 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance *. 30 111’’*1*+’1*++1’’I’+ 7.80 8.00 8.20 8.40 8.60 5000 m/ z 4! .05 10.84%

15 27 41 44 56 87 m/z-__5 Abundance 1"11 ‘ " i ■ “ ■ i ‘‘ i ■ • ■' i" ■ ■ i" ■11" " ।'111111111" i'"111"1111111" " i" " i11" i"111" 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 30 #292: N-Ethylformamide ........................... ...... ' i ‘ ' ■ ■ i ■ ■ ■ ■ i ' ' 7.80 8.00 8.20 1. 8.40 8.60 73 m/ z 71.00 7.19% 5000 44 58 27 15 41 mTTH -HHHH ' i ‘■ i “ 11 “ ■ ‘ i ‘ "11" 11—0umnm[T miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 7.80 8.00 8.20 8.40 8.60

1442.D GCMS0208.M Fri Feb 22 09:36:39 2002 Page 1

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