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GCMS analysis results for sample AE02582, April 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE02582 conducted on April 2, 2002.

NYC-WTC_000058474–000058482

Folder label: “GCMS X 3/4/02 A 3/26/02

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Scanned page image, NYC-WTC_000058481
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2602\2582.D Vial: 16 Acq On : 27 Mar 2002 12:34 am Operator: Sample : re-extract fb Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 1-Butanamine, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.13 2.08 ug/1 339611 1,4-Dichlorobenzene-d4 12.26

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Butanaralne, 3-methyl- 87 C5H13N 000107-85-7 9 2 1,3-Dio:^lane, 2-methyl- 88 C4H8O2 000497-26-7 9 3 N-Ethyhformamide 73 C3H7NO 000627-45-2 9 4 Silane/ tetramethyl- 88 C4H12Si 000075-76-3 9 'Abundance Scan 336 (8.133 min); 2582.D (-) m/ z 73.0^^100.00% 7|3

5000 43

87' 103 7.80 8.00 8.20 810 .......... 3^|l| I 50 55. . , I m/ z 43.05 28.50% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62884: 1-Butanamine, 3-methyi- 3

5000 7.80 8.00 8.20 8.40____ m/z 41.05 10.18% 41 55 87 I ' ' ‘ ' I ' ' ''' '' ' ' ' I'' ' ' ' m/z-> 10 20l 30 40!50 60 70 80 90 100 110 'Abundance #62902: ,3-Dioy.clane. 2-methvl- 73 -- ' ' I .___ Mi--:- 7.80 8.00 8.20 8.40 5000 43 m/ z 10.02%' 58 87 27 ' ' I ‘ ' I ‘ ' I ' ' ' ' I m/z-> 10 . 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethyiformamide 3)0 7.80 8.00 8.20 8.40_____ 73 m/ z 7.30% 5000 44 58

I ' ' ‘ ' I ...... m/2-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 J

2582.D GCMS0308.M Thu Mar 28 16:24:32 2002 Page 1

NYC-WTC_000058481

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NYC-WTC_000058481Source: NYC Law Department, mirrored locally

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