GCMS analytical results for sample AE03828, March 29, 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\MAR2202\3828.D Vial: 9 Acq On : 23 Mar 2002 1:59 am Operator: Sample : gc/ms scan 2/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L

Peak Number 1 1-Butanamine, 3-methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.16 0.38 ug/1 43571 1,4-Dichlorobenzene-d4 12.26

Hit# of 5 Tentative ID MW MolForm CAS# Qual j ' / 1 1-Butanamine , 3-methyl- 87 C5H13N 000107-85-7 9 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 2-Methyl-5-hexen-3-ol 114 C7H140 032815-70-6 9 4 Butane, 2-methoxy-2-methyl- 102 C6H140 _________ 000994-05-8 9 Abundance Scan 339 (8.155 min): 3828.D (-) m/z 73.00 100.00% 73

5000 43 — TT 7.80 8.00 8.20 8.40______

m/z-> 10 20 30 uLL51 4050 60 70 , 87 l • • i • ■ ■'■ i • ■ ■ ■ ।

80 90 100 103 ■

110 i ■ m/z 42.95 30.77% Abundance #763: 1-Butanamine, 3-methyl- 30

5000 -... M 7.80 m/z 8.00 41.05 8.20 TTPr 8.40____ 13.07% :m/z--> 10 15 20 430 41 . 55 Ii ■ ■ ■ Tr ■ । ‘ * —IT 1IIIIII 70 87 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide 3.0 73 - II —-A 7.80 8.00 8.20 8.40______ 5000 m/z 44.9,5 10.75% 44 '58

15 i ■ ' 1 ' i ■ ' ■ ■ I i ■ ■ ■ ■ i ' ■ ■ ■ i ■ ■ ■ ■ i ■ 1 1 1 i ‘ 1 ■ ■ i ■ ■ TIT । । > । । । । । । । । m/z-> 10___20 30 40 50 60 __ 70 80 90 100 110 Abundance #3017: 2-Methyl-5-hexen-3-ol 73 Al TTT । . 7.80 8.00 8.20 8.40_____ 55 m/z 71.00 8.81% 43 5000-

27

m/z-> 10 | | I 1 ' ' ■ i ' ■ • ■ i 1 1 1 1 1 1,1 20 30 . 40 l | . I .’.'I’, 50 60 TT 70 „81 80 90 100 110 7.80 8.00 8.20 8.40

3828.D GCMS0308.M Tue Mar 26 14:57:07 2002 Page 1

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