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GCMS analytical results for sample AE03828, March 29, 2002

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Laboratory report listing detection results for volatile organic compounds in sample AE03828 analyzed on March 29, 2002.

NYC-WTC_000038054–000038063

Folder label: “GCMS X 2/20/02 A 3/22/02

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\MAR2202\3828.D Vial: 9 Acq On : 23 Mar 2002 1:59 am Operator: Sample : gc/ms scan 2/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method C:\HPCHEM\1\METHODS\GCMS0308.M (RTE Integrator) Title 209 625/TCLP calibration table Library C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

14.86 0.70 ug/1 106740 Naphthalene-d8 15.90

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasiloxane/ decamethyl- 370 C10H3005Si5 000541-02-6 53 2 Benzeneethanamine, N- [ (pentafluorop 475 C21H26F5NO2Si2 055429-85-1 38 3 Phenethylamine,/N-methyl-.beta.,3,4 399 C18H37NO3Si3 010538-85-9 32 4 Benzoic acid, -[(trimethylsilyl)ox 282 C13H2203Si2 003789-85-3 28 Abundance Scan 1069 (14.857 min): 3828.D (-) m/z 73.00 100.00% 73

5000 267 355.

: 45 14.60 14.80 15.00 15.20 103 125 1 54 177 193 . 223 251 323 339 : i 1 d ir 1 IIPummmnpu ' I'''') ’ m/z 267.00 38.92% m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73 355 267 5000 T1 14.60 14.80 15.00I 15.20 m/z 355.0 31.71% 191 207 251 323 339 | rrp . , , j , i1'1' i'11' i ‘'111'111 r '1 * i11 ■1 r 1111 i■r 'i TTTTTTTTT TTTTTTT TT m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74573 Benzencethanamine, N-I (pentafl rophsi ry! irnethyenc] 73 7 \ !• ‘ 1 ‘ i 14.60 14.80 15.00 15.20 5000 11.53% 267 44 151 179194209 250 ''I1•1'I1 । ri rrj r. ri । i' TT i11'11 ‘1,1 r *1 * i i •''' i , rr> i । r. । . । > TTTT’TTTT m/z-? 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74239: Phenethylamine, N-methyl-.beta.,3,4-tns(trimethyls . . । . । < । j . I ' 1 I ' ' ' ' I ' ' 73 _____ 14.60 14.80 15.00 15.20 m/z 267.90 10.31% 5000- 355 44 ( 88 130 147 193 267 294 L TI‘ TT 11111»TTTTT TT . r. । Tr f 17 । ITTTTTTT | 1 1 1 * | TTTTT m/z- 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.60 14.80 15.00 15.20

3828.D GCMS0308.M Tue Mar 26 14:57:12 2002 Page 2

NYC-WTC_000038062

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NYC-WTC_000038062Source: NYC Law Department, mirrored locally

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