GCMS blank analysis results, February 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN1502\LB.D Vial: 4 Acq On : 15 Jan 2002 12:52 pm Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 1-Butanamine, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.44 5.20 ug/1 1091560 1,4-Dichlorobenzene-d4 11.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1-Butanamine/ 3-methyl- 87 C5H13N 000107-85-7 9 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 1,3-Dioxolane, 2-methyl- 88 C4H802 000497-26-7 9 4 Pentane,/3-methoxy- 102 C6H140 036839-67-59 Abundance Scan 261 (7.443 min): LB.D (-) m/z 73.00 100.00% 73

5000 43 1***1}***I*‘‘‘I‘-TII44I 38 |, | 50 5,5. 60 67, । , 87 103 7.00 7.20 7.40 7.60 7.80 • ‘ i ' ■ ■ ■ i ■ ' ■ • i ■ TIN dt/*t .■ r‘t . ■ . । । । f » t • ■ । । ■ ■ • । । i'i । । । । m/z 43.00 33.10% miz-? 10 20 30 40 50 60 70 80 90 100 110 Abundance #763: 1-Butanamine, 3-methyl- 30

5000 1****1*‘‘‘I**‘I* rnd ■ ■ 7.00 7.20 7.40 7.60 7.80 m/z 41.00 11.51% 15 41 55 70 87 ' ' i ‘ ‘ I ‘ ' iki s’ 1 ■ •' i 1 ' i • ■ • ■ I ■ • ■ ■ i • 1 1,1 I 1 1 ' 1 I ' ' 1 ' 1 1 miz-> 10 20 30 40 50 .. 60 70 80 90 100 110 Abundance 30 73 f । । । i IItT" ■j-r-r 7.00 7.20 7.40 7.60 7.80 5000 m/z 44.9,5 11.51% 44 58 15 ! 18//1/k/8/B/8/1-E—0—B—ER-T-RI-R/2TT//1-1111II2I11TIIII miz-> 10 20 30 40 50 60 70___80___ 90__ 100 110 Abundance #62902:1,3-Dioxolane. 2-methyl- -Tn"* ,Prr I(s run ' ■ ■ 73 7.00 7.20 _ 7.40 7.60 ■ 7.80 m/z 71.00 6.97% 5000 43 58 27 87 — ———————— TTT i 1 ‘ ' ■ I ‘ ' i ■ • ' ■ i 1 ■ ■ ‘ i ■ 1 • • i ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.00 7.20 7.40 7.60 7.80

LB.D GCMS1126.M Mon Feb 04 15:12:33 2002 Page 1

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