GCMS analysis log for sample AD30605, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C: \HPCHEM\ 1 \DATA\DEC3101\30605.D Vial: 30 Acq On 1 Jan 2002 5:03 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library- : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1-Butanamine, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.61 3.85 ug/1 986083 1,4-Dichlorobenzene-d4 11.67

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 2 N-Ethylformamide 73 C3H7NO 000627-45-2 9 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 4 Penta: , 3-methoxy­ 102 C6H140 036839-67-5 9 Abundance / Scan 279 (7.608 mln): 30605.D (-) m/z 73.00 100.00% 73

5000 43 TP—mnmmmmmm 1 i 1 ‘ 87 103 7.20 7.40 7.60 7.80 8.00 38 |, | 50 55, 60 67, 1 1‘‘ITT-1* TIHTst 4, ■ i * 1 i 1 ■ 1 1 i 11 m/z 43.0.0 32.44% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #763: 1-Butanamine, 3-methyl- 30 % ____________ ______________ 5000 । ‘ ।111 • । < ■ ■ * । ■ ■ ■ • । • ■ 7.20 7,40 7.60 7.80 8.00 m/z 41.05 11.77% 15 1 41 55 70 87 1111** - ‘ IE ■ i ■ ‘‘ ‘ i ■ ■ ■ ' I 1 ' ■ ■ i ■ • i • 1 ■ ' i • ■ ■ • i ■ m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #292: N-Ethylformamide 30 73 7.20 ' 7.40 7.60 7.80 8.00 5000 m/z 45.05 11.60% 44 58

15........ ...... ....... L....................... miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #62932: Silane, tetramethyl- T u '1-1 7. nI"I r । i i ! 73 7.20 7.40 7.60 7.80 8.00 m/z 71.0.0 7.13% 5000

45 15 53 59 88 1I**gI TTT ■ 1 i ■ ■ ■ • i ■ • 1 ■ i 1 ■ ■ • i ' !~ ‘ ‘ . "I ' • • < l ■ ■ • ■ j ‘ • . , ( . . m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80 8.00

30605.D GCMS1126.M Wed Jan 23 08:28:28 2002 Page 1

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