GCMS analysis results for sample AD31456, Feb 2002

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Laboratory report documenting GCMS analysis of sample AD31456 conducted on February 13, 2002.

NYC-WTC_000018039–000018047

Folder label: “GCMS X ? A 1/1/02 1/9/02 12/13/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \HPCHEM\1\DATA\JAN1602\31456.D Vial: 10 Acq On : 16 Jan 2002 8:26 pm Operator: 209 GALOS Sample : gc/ms scan 12/27 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1-Butanamine, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.45 4.07 ug/1 963658 1,4-Dichlorobenzene-d4 11.49

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 2 Pentane, 3-methoxy- 102 C6H140 036839-67-5 9 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 4 1,3-Dioxolane, 2-pentadecyl - 284 C18H36O2 004360-57-0 9 Abundance Scan 262 (7.446 min): 31456.D (-) m/z 73.00 100.00% 73

5000 43 1 1 i 1 1 . . । . . . . । i rr-r| i i 7.20 7.40 7.60 7.80 i 0-10T 1, 1 38.1,.1 50 55, 60.67, , 87 | | I I i r | ■ i’i ri '| i i i i [ > 1TPTIITI 193 m/z 43.05 32.74% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #763: 1-Butanamine, 3-methyl- 30 -- 5000 7.20 7.40 7.60 7.80 m/z 44.95 11.89% 15 41 87 m/z-> ■ ' I ' 10 ■ I ‘ ■ 20 1 30r1 1 1 ’401 1 ' 50 55 60 ' i 1 ' ■ ■ i ‘ 70 70 ■ I ■ ■ ■ ■ i ■ ■ ■'■ i ■ ■ • ■ i ■ ■ ■ ■ i ■ ' 80 90 100 110 Abundance ‘92: Psntsnc -methoxy- 73 » . < r। i * . . । । । j . n . । . . . 7.20 7.40 7.60 7.80 5000 m/z 41.0,0 11.84% 45

27 33 39 55 I m/z-> 1 ‘ i ■ • • ■ i 1 ■ ■ ■ i ■ ■ • ■ I ' ■ ■ ■ i ■ ■ • • i 1 1 1 ' I 1 1 1 ' I ' 1 1 1 I ' 1 ' 1 I 1 1 1 1 i 1 1 10 20 30 40 50 60 70 80 90 100 110 Abundance #845; Silane, tetramethyl- 73 7.20 7.40 7.60 7.80 m/z 71.0,0 6.77% 5000

4.5 15.. 31 ' ‘ I ' ‘ ‘ ‘ I ‘ .... . ' 1 I ' 1 1 1 I 1 1 1 1 I 1 'i I | i i i i | I 88 ■ ■ i ' ' • 1 i ■ * ■ ■ t ■ ■ ■ ■ i ‘ ■ miz-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.607.80

31456.D GCMS0103.M Thu Feb 07 09:17:26 2002 Page 1

NYC-WTC_000018046

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NYC-WTC_000018046Source: NYC Law Department, mirrored locally

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