GCMS analysis comments for sample AD28691, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC0401\28691.D Vial: 11 Acq On 4 Dec 2001 10:08 pm Operator: 209 GALOS Sample gc/ms 11/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1-Butanamine, 3-methyl- Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T.

7.66 0.42 ug/1 95862 1,4-Dichlorobenzene-d4 11.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 2 Silane, tetramethyl- 88 C4H12Si 000075-76-3 9 3 1, 4-Butanediamine 88 C4H12N2 000110-60-1 7 4 1 - Pentanamine 87 C5H13N 000110-58-7 7 Abundance Scan 285 (7.661 min): 28691 .D (-) m/z 73.00 1 00.00% 73

5000 43 7.40 7.60 7.80 8.00 38, 48‘ | 1 r | 57 . . ■ • । | | • ■ ■ » । iii»| 87 ‘ । ■ 103 m/z 43.05 27.62% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #763:1-Butanamine, 3-methyl- 33

5000 • A A , -44 , — A , — 7.40 7.60 7.80 8.00 m/z 41.05 11.53% 41 15 ■ ■ l ■ ■1 ■ ■ l ■ ■ L 55 70 1 ' —4 । ■ . ............. । । । । । । । । ■ ■ i • 87 ■ •‘> I ■ ■ ■ ■ i ■ ■ ■ ■ i ■ mz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #845: Silane, tetramethyl- 73 aAMMAA-C—PMAAL 7.40 7.60 7.80 8.00 5000 m/z 44.95 9.05%

45 15 31 | 55 |............. 88............................. IIT ■'■‘■'I । । । । । । miz—> 10 20 30 40 50 60 70 80 90 100 110 Abundance 33 #62931:1,4-Butanediamine ............. —ea ■ A A ■ ■ । > 7.40 7.60 7.80 8.00 m/z 71.00 I6.57% 43 5000 59 71

m/z—> ' 1 1 1 1 ' ' ! ' ' 10 20 ll 30 40 50 60 J 70 80 —88 90 100 110 7.40 7.60 t

7.80 8.00

28691.D GCMS1126.M Thu Dec 06 13:26:31 2001 Page 1

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