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GCMS analysis log for sample AD30605, Jan 2002

Machine-extracted title · confidence 100%

Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.

NYC-WTC_000018194–000018213

Folder label: “GCMS X 12/27/01 A 1/16/02

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Scanned page image, NYC-WTC_000018202
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NYC 9/11 Public Portal Document Library Search Compound Report Data File C:\HPCHEM\1\DATA\DEC3101\30605.D Vial: 30 Acq On 1 Jan 2002 5:03 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Pentene, 2-methoxy­ Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 7.75 0.65 ug/1 167564 1,4-Dichlorobenzene-d4 11.67 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentene, 2-methoxy- 100 C6H120 061142-47-0 10 2 2,3-Butanedione, monooxime 101 C4H7NO2 000057-71-6 9 3 2-Heptanone 114 C7H14O 000110-43-0 9 4 2-Hexanone, 5-methyl - 114 C7H140 000110-12-3 9 Abundance Scan 295 (7.755 mln): 30605.D (-) m/z 4 .00 100.00%! 43

5000

59 'ri I 1 r 101 . 125 7.40 7.60 7.80 8.00 _______________ 36,, , 49 . 1. 72 82. ■ I . . II]-.'. । . fl i i r-j I’i 11 ■ ■ • ■ t i I ■ • > • । • •117 Ii miz-> 1 ■ i'' • ■ i 1 ■ ■' i ‘' 111 1 • • ।»ill । ■ • m/ z 59.05 13.60 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #1570:2-Pentene, 2-methoxy- 43 55 72 85 i

5000 100 2//14I . .'I . . . . p , , . j . 7.40 7.60 7.80 8.00 m/z 124.8,5 8.86 i I lil ’*!+’’I+**I*I* ’ 1**’I4* ‘ ' l 1 — m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #1697: 2.3-Butanedione, monooxime 43 ............. HA............. ■11 ■ ■ ■' 11 ■' ■ । ■ 111111 ■ ।' 7.40 7.60 7.80 8.00 5000 m/z 127.0,0 6.09

15 101 30 51 58 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 Abundance #64165:2-Heptanone 11/1//-///-/1/5/*/*/-1/n//n//o/t/t/1.B 43 7.40 7.60 7.80 8.00 m/z 101.05 5.74? 58 5000

71

m!z~> 1 d’l 1 ■ ■ I ■ ' 10 20 30 40 50 60 70 85 90 99 ’1’11111111111111 TPTgo 80 100 110 114 120 130 —AAMAA— 7.40 7.60 7.80 8.00 1 1 i ■

30605.D GCMS1126.M Wed Jan 23 08:28:33 2002 Page 2

NYC-WTC_00001 8202

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NYC-WTC_000018202Source: NYC Law Department, mirrored locally

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