GCMS analysis results for sample AD31074, Jan 2002

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Laboratory report documenting GCMS analysis of sample AD31074 conducted on January 18, 2002, noting no unusual compounds were detected.

NYC-WTC_000017405–000017433

Folder label: “GCMS X 12/20/01 A 1/8/02”

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NYC 9/11 Public Portal Document

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Data File C:\HPCHEM\1\DATA\JAN0 802\31074.D Vial: 12 Acq On 9 Jan 2002 12:04 am Operator: 209 GALOS Sample gems scan 12/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

7.46 5.21 ug/1 1379330 1,4-Dichlorobenzene-d4 11.52

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 28 2 Pentane ,/3-methoxy- 102 C6H140 036839-67-5 25 3 l-Butapamine, 3-methyl- 87 C5H13N 000107-85-7 9 4 N-Ethylformamide 73 C3H7NO 000627-45-2 9 Abundance7 Scan 264 (7.465 min): 31074.D (-) m/z 73.00 100.00% 73

5000 43 . ......... a . 12114.4 87 7.20 7.40 7.60 7.80 ■ ■ i ■ ■ ■ ■ i ■ ■ ■ ‘ i ■ -374411r , 55,61 .671 + ■ i ' ' i ■ • ■ ■ । ■ 103 126 1I 1111I1'1 1111 m/z 43.00 33.47% m/z-> . . 10__ 20 30 _ 40.. 50.. 60 70 80 90 100 110 120 130 Abundance #63573: 3-Pentanol, 3-methyl- 73

5000 A 7.20 7.40m - 7.60 7.80 , 55 m/z 41.00 11.97% 9 45 87 '......... 2739 | ■ I ■»i • <»• i ■ ■ ■ ■ i < < < ■ । ■ ■ ■ । ■ ■ ■ । । ■ 1 ■ ■ i ■ • ■' i ■' ■ ■ i • • ■ ■ i ■ ■ ■ ■ i ■ ■ • ■ i ■ ■ mrz-> 10 20 30___ 40 50 60 70 80 90 100 110 120 130 Abundance 73 ; । । vr. T///i । tt i । ia 'i । 7.20 7.40 7.60 7.80 5000 m/ z 45.0,0 11.04% 45

27 33 39 55 ‘ 1 i ■ ■ ■ • i 1 ■ ■ ■ i ■ 1 1 1 i 1 ■ ■ 1 1 ■ 1 1 1 i ■ 1 1 1 1 1 ■ 1 ■ i ■ ■ ■ 1 i 1 1 ■ ■ i 1 ■ • ■ i ■ ‘ ' ■ i ■ ■ 1 1 i 1 m/z-> 10_ 20__ 30__ 40_ 50 60 70 80 90 100 110 120 130 Abundance #763:1-Butanamine, 3-methyl- ... . 30 7.20 7.40 7.60 7.80 m/z 71.00 7.27% 5000

m/z~> ■ ■ i ■ 10 15 ■ i ■ ■ 20 41 — ■ i ■ 55 1 । 30 40 50 60 70 ' 1 i 1 ■ ■ ■ i ■ ■ 70 80 87 90 । ■ ■ ■ ■ । ■ ■ • ■ । ' ■ • ■ । ■ ■ ■ • । 100 110 120 130 ■ A 7.20 7.40 7.60 7.80

31074.D GCMS0103.M Wed Jan 09 12:24:15 2002 Page 1 | NYC-WTC_000017413

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GCMS analysis results for sample AD31018, Jan 2002 · Box DEP Box 16

NYC-WTC_000017380

Laboratory report documenting GCMS analysis of sample AD31018 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.

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