GCMS calibration table review, Jan-Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\JANO802\31344.D Vial: 11 Acq On 9 Jan 2002 11:33 pm Operator: 209 GALOS Sample gems scan 12/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.46 3.02 ug/1 872009 1,4-Dichlorobenzene-d4 11.53

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 36 2 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 3 Silane, tetramethyl- 88 C4H12S1 000075-76-3 9 4 Pentane, 3-methoxy- 102 C6H140 036839-67-5 9 Abundance Scan 264 (7.464 min): 31344.D (-) m/ z 73.00 1 00.00% 73

5000 43

87 103 7.20 7.40 7.60 7.80 3? | 50 55, 60 67, 1 , ■ ■ i ■ • • ■ i • ■ ' ■ i 1 • ‘ 1 I1 11 • i ‘-l 1 1 i 1 1 1 ' l ' i • • i • >»'■ । * * > * । *' * t i । » m/z 43.05 33.79% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63572: 3-Pentanol, 3-methyl- 73

5000 IT 1in ]-1111 55 7.20 7.40 7.60 7.80 45 87 m/z 45.05 12.17%

m/z->____ 10 20 ..... 30 40 1.. 50 #PPP +11—9———0m— 60 70 80 90 100 110 Abundance 4763 1-Batanamine 3-methyl- 30 ■ ■ ■ ■ r 114i । 12— I-, ■ । । 7.20 7.40 7.60 7.80 5000 m/z 41.05 11.94%

15 41 55 70 87 ■ ■ i ' ■ ' ■ i ' ' ‘ ■ i ■ ■ ■ • i • 1 ■ ■ i ■ ■ 1 ■ i ■ • ■ ■ i ■ ■ ■ • i ■ 1 i ■ i 1 1 ' 1 i ' m/z-> 10 20 30 40। 50 60 70 80 90 100 110 Abundance :#62932: Silane, tetramethyl- * "i"! r । [t TI"T j { i i i ITri i r i i 73 7.201 7.40 7.60 7.80 m/z 71.00 6.95% 5000

45 15 I 53 59 88 — ————————— । > I I I'l । । I'i'fi’j i । i > । i **I * * 11**1* miz-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80

31344.D GCMS0103.M Wed Feb 06 11:24:45 2002 Page 1

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