GCMS analysis summary, sample AD27288, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\JAN0 802\27288.D Vial: 26 Acq On 9 Jan 2002 3:42 pm Operator: 209 GALOS Sample gems scan 12/20a Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.47 4.19 ug/1 1057650 1,4-Dichlorobenzene-d4 11.53

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol/' 3-methyl- 102 C6H140 000077-74-7 33 2 1,3 -Dioxolane , 2 -methyl - 88 C4H802 000497-26-7 9 3 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 4 Silane/ tetramethyl- 88 C4H12Si 000075-76-3 9 Abundance Scan 264 (7.470 min): 27288.D (-) m/z 73.00 100.00% 73

5000 43

87 103 7.20 7.40 7.60 7.80 ....................................... 38 | 50 55 67, । , F144naa*I*11I ' * ■ i ■ • 1**114*I* m/z 43.00 31.93% miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63572: 3-Pentanol, 3-methyl- 73

5000 CTm——TPm 55 7.20 7.40 7.60 7.80 45 87 m/z 44.95 11.98% 27 | m/z->__ 10 r ' I 1 11 . । . . . ■ i'. . ■ . । 1 ■ • • i • • 20 30 40 50 + 60 70 I । • I • 80 90 । ... । i । i । । । । 100 110 Abundance ‘ -Ae thi 73 ■ Tt3t 7*’I .-mi n . . 7.20 7.40 7.60 7.80 5000 43 m/z 41.00 1 0.97% 58 27 87 T414441***I+‘‘‘I‘‘‘‘I‘‘‘‘1+**11‘*‘I‘‘**1****I‘‘‘‘I* miz-> 10 20__ 30 40 50 60 70 80 90 100 110 Abundance #763: 1-Butanamine, 3-methyl- —it । i । i r"r1 ‘ ■ ■ | ■ ITTT7 r i i 33 7.20 7.40 7.60 7.80 m/z 71.00 6.92% 5000

41 15 ■ i ‘ ‘ -- 55 70 87 1 ■ i ■ ■ i ■ । . . . . | . . . . । । . i . . . . । . . , । ,Tt r, . m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80

27288.D GCMS1126.M Mon Feb 04 15:22:49 2002 Page 1

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