GCMS analysis results for sample AD27288, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\JANO802\27288.D Vial: 26 Acq On 9 Jan 2002 3:42 pm Operator: 209 GALOS Sample gems scan 12/20a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

7.47 4.19 ug/1 1057650 1,4-Dichlorobenzene-d4 11.53

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 33 2 1,3-Dioxolane, 2-methyl- 88 C4H802 000497-26-7 9 3 1-Butanamine, 3-methyl- 87 C5H13N 000107-85-7 9 4 Silane, t ramethyl- 88 C4H12Si _ 000075-76-3 9 Abundance / Scan 264 (7.470 mln): 27288.D (-) m/z 73.00 1 00.00% i / 73

5000 43 • ■ • • । ■ 11 ■ ■ ■ 11. ।. 7.20 7.40 7.60 7.80 1 miz-> ‘ ' I ‘ ‘ 10 ‘ I ‘ 20 ' I ' 30 , 38,11,1, 40 50 — 60 67+ 70 , 80 87 90 ' • • I ‘ • 1 i > • • ■ i 100 I?3 ■ ■ i ■ 110 m/z 43.00 31.93% Abundance #63572:3-Pentanol, 3-methyl- 73

| 5000 ■ ‘ ■ i 1 1 1 r l’ ’ 1 1 1 1 1tmi rr '■ • ' 55 7.20 7.40 7.60 7.80 45 87 m/z 44.95 11.98%

miz-> ... 10 20 3730..40 1.50 60 70 80 1 1 1 I ■ ■ 12**

90 100 110 Abundance #62902: 1,3-Dioxolane. 2-methl- 73 3*5 * . [mm 1‛i 11t7 1111 7.20 7.40 7.60 7.80 5000 43 m/z 41.00 1 0.97% 58 27 87 i —— — — i . ■ 1 i ‘ ‘ ' ■ i • ‘ ' ■ i 1 1 I • ■ ' 1 i • • ' ' i ' ' ' ■ i ‘ ‘ 1 ‘ i • ■ ‘ ■ i ■ miz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #763: 1-Butanamine, 3-methyl- CTTTTTTuTpeu 7.20 7.40 7.60 7.80 m/z 71.00 6.92% 5000

..15.. i, . ■ ■ 1’411’1 l-i j--) 55i' I i । > I I i70x i i —j n 87>' । । > > > i । i r i i j r t • • । ‘ ■ i ' ■ ■ ■ i ■ ■r r i ■ •

miz-> 10 20 30 40 50 60 70 80 90 100 110 7.20 7.40 7.60 7.80

27288.D GCMS0103.M Thu Jan 10 09:36:35 2002 Page 1

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