Laboratory report listing PAHs and phthalates in a water sample scheduled for re-extraction and re-analysis.
NYC-WTC_000018005–000018025Folder label: “GCMS X ? A 1/1/02 1/9/02 12/13/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\JAN0 802\27288.D Vial: 26 Acq On 9 Jan 2002 3:42 pm Operator: 209 GALOS Sample gems scan 12/20a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 5
R.T. EstConc Area Relative to ISTD R.T.
14.17 2.10 ug/1 662556 Naphthalene-d8 15.13
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasil ane, decamethyl- 370 C10H3005Si5 000541-02-6 53 2 N- (Trif luoroa cetyl)-0,0',0'‘-tris(t 481 C19H34F3NO4Si3 000000-00-0 43 3 Benzoic acid, 2-[(trimethylsilyl)ox 282 C13H2203Si2 003789-85-3 38 4 3,4-Dihydroxybenzyl alcohol, tris (tr 356 C16H3203Si3 068595-79-9 38 Abundance 73 Scan 994 (14.172 mln): 27288.D (-) m/ z 73.00 100.00%
5000 267 355 13.80 14.00 14.20 14.40 14.60 45 - 108 133154 i । i i > . j’ 193,223 247 4 293 323 , 1 m/z 267.0,0 36.99% miz-> 50 100 150 200 250 300 350 400 450 Abundance #51266: Cyclopentasiloxane, decamethyl- 73 355 267 11 5000 ■ i ' 1 1 ■ i • ' ■ ■ i‘ ■ ■ ■ i1 1 1‘I' 13.80 14.00 14.20 14.40 14.60 m/z 355.0.5 28.63% i i । 1 i *i » । _ j t । > i , 207 . 323 | ’ i • • » I । ■ i m/z~> 50 100 150 200 250 300 350 400 450 Abundance #58326: N-(Trifuoroacety)-0.O,0"-tris(trimethylsily!)no 73 4I***I**1**‘I**L8 355 13.80 14.00 14.20 14.40 14.60 5000 m/z 268.0,0 10.01%
45 . ■ ■ । 126147 193 265 376 481 • i ‘ ■ i ■ * 1 i ‘ 1 1 1 mz-> 50 100 150 200 250 300 350 400 450 Abundance #72298: Benzoic acid, 2-[(trimethylsilyl)oxy]-, trimethylsi ■ i ' ■ ■ ■ i • ■ • • i 1 ■ 1 ■ i ’ ' 1 ■ I ' 73 267 13.80 14.00 14.20 14.40 14.60 m/z 356.05 9.79% 5000
135 193 233 47 'I 1 1 Z . ................... ■ । ■1 • • ।' ■ • ■ । ■ ■ ■ ■ । • • ■ ■ । ■ miz-> 50 100 150 200 250 300 350 400 450 13.80 14.00 14.20 14.40 14.60
27288.D GCMS0103.M Thu Jan 10 09:36:40 2002 Page 2
NYC-WTC_000018014
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NYC-WTC_000016096
GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018174
Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017380
Laboratory report documenting GCMS analysis of sample AD31018 conducted on January 18, 2002, showing detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018693
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036656
Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000017980
Document with unreadable text from the GCMS X folder series in DEP Box 16.
Filed in the same folder
NYC-WTC_000017981
Laboratory notes regarding GCMS scan results and recovery rates for sample AD25874 dated January 18, 2002.
Filed in the same folder
NYC-WTC_000017989
Gas chromatography-mass spectrometry analysis of sample AD26011 from January 18, 2002, detecting 2-(2-ethoxyethoxy)ethanol and 2-ethoxybutane with no blank contamination.
Filed in the same folder
NYC-WTC_000017997
Laboratory report noting detection of 1,1,2,2-Tetrachloroethane in a water sample with no other non-target compounds.
Filed in the same folder
NYC-WTC_000018026
Laboratory report documenting GCMS analysis of sample AD28968 conducted on January 9, 2002.
Filed in the same folder